Hydrothermal Synthesis of Carbon Microspheres from Glucose: Tuning Sphere Size by Adding Oxalic Acid

被引:17
|
作者
Liu, Jie [1 ]
Tian, Peng [1 ]
Ye, Junwei [1 ]
Zhou, Li [1 ]
Gong, Weitao [1 ]
Lin, Yuan [1 ]
Ning, Guiling [1 ]
机构
[1] Dalian Univ Technol, Sch Chem Engn, State Key Lab Fine Chem, Dalian 116012, Peoples R China
关键词
D O I
10.1246/cl.2009.948
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Carbon spheres were successfully prepared via hydrothermal treatment of glucose, and spherical size (0.5-8 mu m) could be tuned by adding different amount of oxalic acid. The surface of obtained carbon spheres contains hydrophilic functionalities including -OH, -C=O, and COOH groups, which were not destroyed by oxalic acid. This Study provided a facile, simple route for producing size-tunable carbon microspheres with functional groups.
引用
收藏
页码:948 / 949
页数:2
相关论文
共 50 条
  • [21] Studies on the sorption of Pu(IV) on alumina microspheres from nitric acid - oxalic acid solutions
    Pius, IC
    Bhanushali, RD
    Pillai, KT
    Mukerjee, SK
    Vaidya, VN
    JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY, 1999, 240 (03) : 981 - 985
  • [22] Scalable Synthesis of Uniform Mesoporous Aluminosilicate Microspheres with Controllable Size and Morphology and High Hydrothermal Stability for Efficient Acid Catalysis
    Li, Yunqing
    Zhang, Xiangcheng
    Shang, Chao
    Wei, Xiangru
    Wu, Lei
    Wang, Xiaoning
    Wu, Winston Duo
    Chen, Xiao Dong
    Selomulya, Cordelia
    Zhao, Dongyuan
    Wu, Zhangxiong
    ACS APPLIED MATERIALS & INTERFACES, 2020, 12 (19) : 21922 - 21935
  • [23] Hydrothermal Synthesis of Nanodisperse V2O5 Using Oxalic Acid
    Gorobtsov, F. Yu
    Simonenko, T. L.
    Simonenko, N. P.
    Simonenko, E. P.
    Sevastyanov, V. G.
    Kuznetsov, N. T.
    RUSSIAN JOURNAL OF INORGANIC CHEMISTRY, 2022, 67 (07) : 1094 - 1100
  • [24] Facile synthesis of hydroxyl aluminum oxalate based on the hydrothermal reaction of boehmite and oxalic acid
    Chen, Haiyang
    Ren, Bo
    Liu, Meng
    Qin, Tingwei
    Guo, Qiang
    Li, Guangqi
    Gong, Diansheng
    Cheng, Guanglin
    Chen, Junhong
    Li, Bin
    COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2022, 639
  • [25] Hydrothermal Synthesis of Nanodisperse V2O5 Using Oxalic Acid
    F. Yu. Gorobtsov
    T. L. Simonenko
    N. P. Simonenko
    E. P. Simonenko
    V. G. Sevastyanov
    N. T. Kuznetsov
    Russian Journal of Inorganic Chemistry, 2022, 67 : 1094 - 1100
  • [26] Synthesis of carbon spheres from glucose using the hydrothermal carbonization method for the fabrication of EDLCs
    Tovar-Martinez, E.
    Sanchez-Rodriguez, C. E.
    Sanchez-Vasquez, J. D.
    Reyes-Reyes, M.
    Lopez-Sandoval, R.
    DIAMOND AND RELATED MATERIALS, 2023, 136
  • [27] SYNTHESIS OF OLIGOESTERS FROM OXALIC-ACID AND GLYCEROL
    ALKSNIS, AF
    GRUZIN, IV
    SURNA, YA
    JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY, 1976, 14 (11) : 2631 - 2638
  • [28] Electrochemical Synthesis of Glycine from Oxalic Acid and Nitrate
    Kim, Jeong Eun
    Jang, Jun Ho
    Lee, Kyu Min
    Balamurugan, Mani
    Jo, Young In
    Lee, Moo Young
    Choi, Seungwoo
    Im, Sang Won
    Nam, Ki Tae
    ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2021, 60 (40) : 21943 - 21951
  • [29] Hydrothermal Separation of Titanium Vanadium and Chromium from a Pregnant Oxalic Acid Leachate
    Dong, Zihui
    Zhang, Jie
    Yan, Baijun
    MATERIALS, 2022, 15 (04)
  • [30] Synthesis of carbon micro-spheres by a glucose hydrothermal method
    Mi, Yuanzhu
    Hu, Weibing
    Dan, Youmeng
    Liu, Yingliang
    MATERIALS LETTERS, 2008, 62 (8-9) : 1194 - 1196