Synthesis and Characterization of a Novel Two-Dimensional Network Polymer Containing 18-and 26-Membered Organotin Macrocycles

被引：6

作者：

Wang, Qingfeng ^{[1
]}

Zhang, Jianping ^{[1
]}

Han, Yinfeng ^{[1
]}

机构：

[1] Taishan Univ, Dept Chem, Tai An 271021, Shandong, Peoples R China

来源：

HETEROATOM CHEMISTRY | 2016年 / 27卷 / 01期

关键词：

CRYSTAL-STRUCTURE; STRUCTURAL CHEMISTRY; X-RAY; CARBOXYLATES; ASSEMBLIES; COMPLEXES; ACID; NMR;

D O I：

10.1002/hc.21285

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The reaction of 4-mercaptophenylacetic acid with dimethyltin dichloride in the presence of sodium ethoxide in ethanol affords a novel two-dimensional organotin network structure compound 1, which is an unusual network containing dinuclear 18-membered and tetranuclear 26-membered organotin macrocycles. The compound has been characterized by elemental analysis, IR, and H-1, C-13, and Sn-119 NMR spectroscopy. Furthermore, we have also characterized the compound by X-ray crystallography. (C) 2015 Wiley Periodicals, Inc.

引用

页码：32 / 36

页数：5

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