Synthesis, Structural Characterization, and Thermal Stability of Di-n-butyltin (IV) Carboxylate Containing a Sn2O2 Ring

被引：3
|
作者：
Liu, Chun-Ling [1 ]
Zhu, Dong-Sheng [2 ]
Li, Chuan-Bi [1 ]
机构：
[1] Jilin Normal Univ, Coll Chem, Minist Educ, Key Lab Preparat & Applicat Environm Friendly Mat, Siping, Peoples R China
[2] NE Normal Univ, Dept Chem, Changchun 130024, Peoples R China
来源：
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2016年 / 46卷 / 08期
基金：
中国国家自然科学基金;
关键词：
1D chain; thermal stability; organotin carboxylate; CRYSTAL-STRUCTURES; DERIVATIVES; ACID; COMPLEXES; TIN; CHEMISTRY; LIGAND;
D O I：
10.1080/15533174.2015.1004457
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The reaction of di-n-butyltin (IV) oxide with 2,4-dichlorobenzylideneaminooxy acetic acid (HL) yielded the organotin carboxylate {[(C4H9)(2)Sn(L)](2)O}(2) (1). The complex was characterized by elemental analysis, FT-IR, NMR (H-1, C-13) spectroscopy and single-crystal X-ray diffraction. The structural analysis showed that complex 1 was a typical ladder framework and further interlinked by intermolecular C-H center dot center dot center dot O hydrogen bonds into a 1D chain. The thermal stability was also investigated.
引用
收藏
页码：1272 / 1276
页数：5
相关论文
共 50 条
  • [21] INVITRO ANTITUMOR ACTIVITIES OF A NOVEL 2/3 CONDENSATION PRODUCT OF SALICYLALDOXIME WITH DI-N-BUTYLTIN(IV) OXIDE
    BOUALAM, M
    BIESEMANS, M
    MEUNIERPIRET, J
    WILLEM, R
    GIELEN, M
    APPLIED ORGANOMETALLIC CHEMISTRY, 1992, 6 (02) : 197 - 205
  • [22] Synthesis and crystal structure of di-n-butyltin(IV) complex with 2-oxo-propionic acid (4-pyridinecarbonyl) hydrazone
    Liu, HW
    Lu, WG
    Tao, JX
    CHINESE JOURNAL OF CHEMISTRY, 2004, 22 (01) : 109 - 113
  • [23] Synthesis, spectral characterization and crystal structure of a novel trinuclear di-n-butyltin(IV) complex with pyruvic acid-N(4)-cyclohexylthiosemicarbazone (H2PACT)
    Salam, M. A.
    Affan, M. A.
    Ahmad, Fasihuddin B.
    Jusoh, I.
    Shamsuddin, Mustaffa B.
    Yamin, Bohari
    Farina, Yang
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2012, 696 (26) : 4202 - 4206
  • [24] PYROLYTIC PROPERTIES OF DI-N-BUTYLTIN(IV) DIACETATE AS A PRECURSOR FOR SPRAYED SNO2 THIN-FILMS
    YAGI, I
    IKEDA, E
    KUNIYA, Y
    JOURNAL OF MATERIALS RESEARCH, 1994, 9 (03) : 663 - 668
  • [25] Crystal structure of bis[benzyl(methyl) carbamodithioato-κ2 S,S′]-di-n-butyltin(IV), C26H38N2S4Sn
    Abd Aziz, Nurul Amalina
    Awang, Normah
    Chan, Kok Meng
    Kamaludin, Nurul Farahana
    Anuar, Nur Najmi Mohamad
    Jamaludin, Nur Atiyah Nadhrah
    Tan, Yee Seng
    Tiekink, Edward R. T.
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2023, 238 (01): : 15 - 18
  • [26] Di-n-butyltin(IV) derivatives of bis(carboxymethyl)benzylamines:: synthesis, NMR and X-ray structure characterization and in vitro antitumour properties
    Mancilla, T
    Carrillo, L
    Rivera, LSZ
    Camacho, CC
    de Vos, D
    Kiss, R
    Darro, F
    Mahieu, B
    Tiekink, ERT
    Rahier, H
    Gielen, M
    Kemmer, M
    Biesemans, M
    Willem, R
    APPLIED ORGANOMETALLIC CHEMISTRY, 2001, 15 (07) : 593 - 603
  • [27] Microwave Solvothermal Synthesis, Crystal Structures and in Vitro Antitumor Activities of Di-n-butyltin Piperonylate with a Sn4O4 Ladder Framework
    Kuang Dai-Zhi
    Feng Yong-Lan
    Jiang Wu-Jiu
    Zhu Xiao-Ming
    Yu Jiang-Xi
    Zhang Fu-Xing
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2018, 37 (08) : 1265 - 1271
  • [28] Synthesis, Spectral, Thermal and Structural Characterization of Two Complexes Containing [N-(2-Hydroxyethyl)-Ethylenediamine] with Carboxylate
    Aycan, Tugba
    Pasaoglu, Humeyra
    TURKISH PHYSICAL SOCIETY 33RD INTERNATIONAL PHYSICS CONGRESS (TPS33), 2018, 1935
  • [29] Synthesis, characterization of di-n-butyltin compounds with (thiocarbamoylthio) acetic acid and crystal structure of {[n-Bu2Sn(O2CCH2CS2NC5H10)]2O}2•2H2O and n-Bu2Sn(O2CCH2CS2NC5H10)2
    Yin, HD
    Xue, SC
    Wang, QB
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2005, 44 (05): : 1040 - 1045
  • [30] Microwave Solvothermal Synthesis, Crystal Structures and in Vitro Antitumor Activities of Di-n-butyltin Piperonylate with a Sn4O4 Ladder Framework
    邝代治
    冯泳兰
    蒋伍玖
    朱小明
    庾江喜
    张复兴
    Chinese Journal of Structural Chemistry, 2018, 37 (08) : 1265 - 1271
12345