Synthesis, Structural Characterization, and Thermal Stability of Di-n-butyltin (IV) Carboxylate Containing a Sn2O2 Ring

被引：3
|
作者：
Liu, Chun-Ling [1 ]
Zhu, Dong-Sheng [2 ]
Li, Chuan-Bi [1 ]
机构：
[1] Jilin Normal Univ, Coll Chem, Minist Educ, Key Lab Preparat & Applicat Environm Friendly Mat, Siping, Peoples R China
[2] NE Normal Univ, Dept Chem, Changchun 130024, Peoples R China
来源：
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2016年 / 46卷 / 08期
基金：
中国国家自然科学基金;
关键词：
1D chain; thermal stability; organotin carboxylate; CRYSTAL-STRUCTURES; DERIVATIVES; ACID; COMPLEXES; TIN; CHEMISTRY; LIGAND;
D O I：
10.1080/15533174.2015.1004457
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The reaction of di-n-butyltin (IV) oxide with 2,4-dichlorobenzylideneaminooxy acetic acid (HL) yielded the organotin carboxylate {[(C4H9)(2)Sn(L)](2)O}(2) (1). The complex was characterized by elemental analysis, FT-IR, NMR (H-1, C-13) spectroscopy and single-crystal X-ray diffraction. The structural analysis showed that complex 1 was a typical ladder framework and further interlinked by intermolecular C-H center dot center dot center dot O hydrogen bonds into a 1D chain. The thermal stability was also investigated.
引用
收藏
页码：1272 / 1276
页数：5
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