Evaluation of Microwave-Assisted Extraction for the Analysis of Polychlorinated Biphenyls and Organochlorine Pesticides in Fish

被引：0
|
作者：
Otake, Takamitsu [1 ]
Aoyagi, Yoshie [1 ]
Numata, Masahiko [1 ]
Yarita, Takashi [1 ]
机构：
[1] Natl Inst Adv Ind Sci & Technol, Natl Metrol Inst Japan, Tsukuba, Ibaraki 3058563, Japan
来源：
JOURNAL OF AOAC INTERNATIONAL | 2008年 / 91卷 / 05期
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D O I：
暂无
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The efficiency of microwave-assisted extraction (MAE) was evaluated for the analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in fish. An isotope dilution method was used for quantification via analysis of the samples by gas chromatography and mass spectrometry. MAE solvent, temperature, and time were optimized, and observed concentrations were compared. The MAE results were also compared to those of other extraction techniques (Soxhlet extraction, pressurized liquid extraction, saponification, and homogenization). Concentrations of PCBs and OCPs obtained by MAE at 120 degrees C for 10 min were comparable to those by the other techniques. The results suggest that MAE can be used for the analysis of PCBs and OCPs in fish.
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页码：1124 / 1129
页数：6
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