Evaluation of Microwave-Assisted Extraction for the Analysis of Polychlorinated Biphenyls and Organochlorine Pesticides in Fish

被引：0
|
作者：
Otake, Takamitsu [1 ]
Aoyagi, Yoshie [1 ]
Numata, Masahiko [1 ]
Yarita, Takashi [1 ]
机构：
[1] Natl Inst Adv Ind Sci & Technol, Natl Metrol Inst Japan, Tsukuba, Ibaraki 3058563, Japan
来源：
JOURNAL OF AOAC INTERNATIONAL | 2008年 / 91卷 / 05期
关键词：
D O I：
暂无
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The efficiency of microwave-assisted extraction (MAE) was evaluated for the analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in fish. An isotope dilution method was used for quantification via analysis of the samples by gas chromatography and mass spectrometry. MAE solvent, temperature, and time were optimized, and observed concentrations were compared. The MAE results were also compared to those of other extraction techniques (Soxhlet extraction, pressurized liquid extraction, saponification, and homogenization). Concentrations of PCBs and OCPs obtained by MAE at 120 degrees C for 10 min were comparable to those by the other techniques. The results suggest that MAE can be used for the analysis of PCBs and OCPs in fish.
引用
收藏
页码：1124 / 1129
页数：6
相关论文
共 50 条
  • [1] Evaluation of microwave-assisted extraction for the analysis of polychlorinated biphenyls and organochlorine pesticides in fish
    Otake, Takamitsu
    Aoyagi, Yoshie
    Numata, Masahiko
    Yarita, Takashi
    [J]. 2008, AOAC International (91)
  • [2] Evaluation of a microwave-assisted extraction technique for the determination of polychlorinated biphenyls and organochlorine pesticides in sediments
    Numata, M
    Yarita, T
    Aoyagi, Y
    Takatsu, A
    [J]. ANALYTICAL SCIENCES, 2004, 20 (05) : 793 - 798
  • [3] Evaluation of a Microwave-Assisted Extraction Technique for the Determination of Polychlorinated Biphenyls and Organochlorine Pesticides in Sediments
    Masahiko Numata
    Takashi Yarita
    Yoshie Aoyagi
    Akiko Takatsu
    [J]. Analytical Sciences, 2004, 20 : 793 - 798
  • [4] Microwave-assisted steam distillation for simple determination of polychlorinated biphenyls and organochlorine pesticides in sediments
    Numata, M
    Yarita, T
    Aoyagi, Y
    Takatsu, A
    [J]. ANALYTICAL CHEMISTRY, 2003, 75 (06) : 1450 - 1457
  • [5] Microwave-assisted extraction method for organochlorinated pesticides and polychlorinated biphenyls from compost
    Losier, J
    Girard, L
    [J]. INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 2001, 80 (01) : 1 - 11
  • [6] Pressurized liquid extraction in determination of polychlorinated biphenyls and organochlorine pesticides in fish samples
    Suchan, P
    Pulkrabová, J
    Hajslová, J
    Kocourek, V
    [J]. ANALYTICA CHIMICA ACTA, 2004, 520 (1-2) : 193 - 200
  • [7] Pressurized liquid extraction and microwave-assisted extraction in the determination of organochlorine pesticides in fish muscle samples
    Barriada-Pereira, Mercedes
    Iglesias-Garcia, Ivan
    Gonzalez-Castro, Maria J.
    Muniategui-Lorenzo, Soledad
    Lopez-Mahia, Purificacon
    Prada-Rodriguez, Dario
    [J]. JOURNAL OF AOAC INTERNATIONAL, 2008, 91 (01) : 174 - 180
  • [8] Levels of organochlorine pesticides and polychlorinated biphenyls in Baltic fish
    Niewiadowska, Alicja
    Kiljanek, Tomasz
    Semeniuk, Stanislaw
    Zmudzki, Jan
    [J]. MEDYCYNA WETERYNARYJNA-VETERINARY MEDICINE-SCIENCE AND PRACTICE, 2012, 68 (02): : 114 - 118
  • [9] Optimization of a microwave-assisted extraction method for the analysis of polychlorinated biphenyls in ash samples
    Criado, AR
    Pereiro, IR
    Torrijos, RC
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2003, 985 (1-2) : 137 - 145
  • [10] Microwave-assisted extraction versus Soxhlet extraction in the analysis of 21 organochlorine pesticides in plants
    Barriada-Pereira, M
    Concha-Graña, E
    González-Castro, MJ
    Muniategui-Lorenzo, S
    López-Mahía, P
    Prada-Rodríguez, D
    Fernández-Fernández, E
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2003, 1008 (01) : 115 - 122
12345