Influence of TiO2 Incorporation on the Microstructure, Optical, and Dielectric Properties of TiO2/Epoxy Composites

被引:47
|
作者
Bouzidi, A. [1 ,2 ]
Omri, K. [3 ]
Jilani, W. [1 ,4 ]
Guermazi, H. [1 ]
Yahia, I. S. [5 ,6 ,7 ]
机构
[1] Univ Sfax, Fac Sci, Res Unit, Phys Insulating & Semi Insulating Mat, BP 1171, Sfax 3000, Tunisia
[2] Tech & Vocat Training Corp, Tech Coll Branch, POB 10, Ahad Rufidah 61974, Saudi Arabia
[3] Fac Sci Gabes, Lab Phys Mat & Nanomat Appl Environm, Cite Erriadh Manara Zrig 6072, Gabes, Tunisia
[4] King Khalid Univ, Fac Sci Sci & Arts Dhahran Al Janoub, Dept Phys, POB 960, Abha 61421, Saudi Arabia
[5] King Khalid Univ, RCAMS, POB 9004, Abha 61413, Saudi Arabia
[6] King Khalid Univ, Fac Sci, Dept Phys, AFMOL, POB 9004, Abha, Saudi Arabia
[7] Ain Shams Univ, Fac Educ, Dept Phys, Semicond Lab,NLEBA, Cairo 11757, Egypt
关键词
Composites; Microstructure; TiO2; Optical properties; Dielectric properties; THIN-FILMS; STRUCTURAL-PROPERTIES; NANOSIZE RUTILE; QUANTUM DOTS; BAND-GAP; NANOCOMPOSITES; PARTICLES; TRANSPARENT; CONSTANTS; FABRICATION;
D O I
10.1007/s10904-017-0772-9
中图分类号
O63 [高分子化学(高聚物)];
学科分类号
070305 ; 080501 ; 081704 ;
摘要
This study begins with a synthesis and characterization of Epoxy/TiO2 composites (Ep-TiO2-Cs) with different TiO2 fillers. The ultrasonic mixing process was employed to disperse the TiO2 fillers into the epoxy resin matrix. The effect of TiO2 contents on microstructural, optical and electrical properties of the Ep-TiO2-Cs have investigated. Several techniques are now being used to characterize the Ep-TiO2-Cs. The microstructure of fracture surfaces was examined by SEM techniques. It revealed that the as-prepared TiO2 particles are a spherical shape structure. At 5.0 wt% TiO2 fillers, it is evident that these spheres are homogeneously distributed in the epoxy matrix. The XRD study confirms that the particle size generally decreases with increasing the added TiO2 fillers in the epoxy matrix. In the UV-light range, the neat epoxy only blocks UV-light in the range of 200-280 nm, it becomes high UV-light blocker (up to 400 nm) via the addition of TiO2 powder with 5.0 wt% fillers. Moreover, the TiO2 content addition obviously enhanced the UV-Shielding efficiency of the epoxy resin.
引用
收藏
页码:1114 / 1126
页数:13
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