Growth and characterization of non-linear optical crystal Cd3Zn3B4O12

被引：6
|
作者：
Zhang, Fan [1 ]
Shen, Dezhong [1 ]
Shen, Guangqiu [1 ]
Wang, Xiaoqing [1 ]
机构：
[1] Tsinghua Univ, Dept Chem, Beijing 100084, Peoples R China
来源：
MATERIALS RESEARCH BULLETIN | 2008年 / 43卷 / 12期
基金：
中国国家自然科学基金;
关键词：
Optical material; Inorganic compounds; Crystal growth; Optical properties;
D O I：
10.1016/j.materresbull.2008.08.016
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Cd3Zn3B4O12 polycrystals were synthesized by solid-state and wet chemical reaction methods. Cd3Zn3B4O12 single crystals with millimeter grade were grown from the self-flux B2O3 (Cd:Zn:B = 1: 1: 1.5); and larger crystals were obtained from the PbO-0.85PbF(2) fluxes easily. As-grown crystals were characterized by differential scanning calorimetry and thermogravimetric, X-ray diffraction, infrared and Raman spectral analysis, respectively. The non-linear optical coefficient of the Cd3Zn3B4O12 crystal is 2.6 times as large as that of KH2PO4 crystal. Chemical etching shows that this crystal is very stable in neutral solution and not hygroscopic in air at room temperature. Crown Copyright (c) 2008 Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码：3188 / 3194
页数：7
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