Qualitative analysis of volatile compounds in perfumes by headspace solid phase microextraction/gas chromatography-mass spectrometry

被引:0
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作者
Chitsamphandhvej, W [1 ]
Thongoon, W [1 ]
Trirat, P [1 ]
机构
[1] King Mongkuts Univ Technol, Dept Chem, Fac Sci, Bangkok, Thailand
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暂无
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
The volatile components of twenty kinds of perfumes were investigated. These volatile components were obtained by Headspace-Solid Phase Microextraction (HS-SPME) technique with four types of fibers; DVB/CAR/PDMS, CW/DVB, PDMS/DVB and CAR/PDMS. The determination was performed in combination of gas chromatography-mass spectrometry (GC-MS). The result showed that DVB/CAR/PDMS and PDMS/DVB gave better extraction response than CW/DVB and CAR/PDMS. One hundred and thirteen compounds were identified and classified to forty-two alkenes, twenty-six esters, fourteen alcohols, twelve ketones, nine aldehydes, six ethers, three hydrocarbons and two carboxylic acids. The volatile compounds which found in many perfumes were alpha-Pinene, beta-Pinene, beta-Myrcene, Cymene, Limonene, Linalool, Benzyl acetate, Linalyl acetate and Lilial.
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页码:353 / 360
页数:8
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