Preparation and characterization of polymer-supported nano-amorphous Ni-B particles

被引:3
|
作者
Wen, Hong-Liang [1 ]
Yao, Kai-Sheng [1 ]
Wei, Jia [1 ]
Zhou, Zhi-Ming [1 ]
Kirschning, Andreas [2 ]
机构
[1] Beijing Inst Technol, Sch Chem Engn & Environm, Beijing 100081, Peoples R China
[2] Leibniz Univ Hannover, Inst Organ Chem, D-30167 Hannover, Germany
关键词
Nano-amorphous; Polymer-supported; Ni-B; Ion exchange/chemical reduction; Preparation; Nanoparticles; Nanocomposites; ACRYLONITRILE HYDROGENATION; CATALYST; ALLOY; CYCLOPENTADIENE; REDUCTION; POWDER;
D O I
10.1007/s11051-008-9464-2
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Polymer-supported nano-amorphous Ni-B particles have been prepared by an ion exchange/chemical reduction protocol. The products were characterized by inductively coupled plasma spectroscopy (ICP), X-ray powder diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The polymer-supported Ni-B particles prepared at low temperature are 60-70 nm in size with a Ni-B ratio of Ni(19)B(10).The choice of temperature is a crucial factor affecting particle size.
引用
收藏
页码:499 / 503
页数:5
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