Crystal structure of (2S, 4R)-2-benzyl 1-tert-butyl 4-(tosyloxy)pyrrolidine-1,2-dicarboxylate, C24H29NO7S

被引:1
|
作者
Ghosh, Munmun [1 ]
Mallick, Arijit [2 ]
Diaz Diaz, David [1 ,3 ]
机构
[1] Univ Regensburg, Inst Organ Chem, D-93040 Regensburg, Germany
[2] Natl Chem Lab, Phys Mat Chem Div, Pune 411008, Maharashtra, India
[3] Univ Zaragoza, ISQCH, CSIC, E-50009 Zaragoza, Spain
关键词
D O I
10.1524/ncrs.2012.0173
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C24H29NO7S, triclinic, P1 (no. 1), a = 6.5903(3) angstrom, b = 9.7193(5) angstrom, alpha = 82.462(4)degrees, beta = 77.197(3)degrees, gamma = 85.6180(4)degrees, V = 617.7 angstrom(3), Z = 1, R-gt(F) = 0.0351, wR(ref)(F-2) = 0.0967, T = 123 K.
引用
收藏
页码:361 / 362
页数:2
相关论文
共 50 条
  • [32] Synthesis and Crystal Structure of (2S,2'S,4'R)-2-(1-Hydroxy-1-ethylpropyl)-1-[(1'-p-tosyl-4'-hydroxypyrrolidin-2'-yl)methyl]pyrrolidine
    FU Yu-Qin DING Li-Na ZHANG Sheng-Hong TAO Jing-Chao ② ZHU Yu (Department of Chemistry
    Chinese Journal of Structural Chemistry, 2006, (10) : 1203 - 1208
  • [33] Synthesis and crystal structure of (2S,2′S,4′R)-2-(1-hydroxy-1-ethylpropyl)-1-[(1′-p-tosyl-4′-hydroxypyrrolidin-2′-yl)methyl]pyrrolidine
    Fu Yu-Qin
    Ding Li-Na
    Zhang Sheng-Hong
    Tao Jing-Chao
    Zhu Yu
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2006, 25 (10) : 1203 - 1208
  • [34] Crystal structure of dimethyl (R)-2-(3-(1-phenylethyl)thioureido)-[1,1′-biphenyl]-4,4′-dicarboxylate, C25H24N2O4S
    Chen, Yi
    Shi, Da-Bin
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2024, 239 (03): : 569 - 571
  • [35] Synthesis and Crystal Structure of (2S,2'S,4'R)-2-(1-Hydroxy-1-ethylpropyl)-1-[(1'-p-tosyl-4'-hydroxypyrrolidin-2'-yl)methyl]pyrrolidine
    FU YuQin DING LiNa ZHANG ShengHong TAO JingChao ZHU Yu Department of Chemistry New Drug Research Development Center Zhengzhou University Zhengzhou China
    结构化学, 2006, (10) : 1203 - 1208
  • [36] Crystal structure of 1,1,2,2-tetra-tert-butyl-1,2-dichlorodisilane, [(C4H9)2ClSi]2
    Peters, K
    Peters, EM
    Kirmaier, L
    Weidenbruch, M
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 1998, 213 (04): : 747 - 748
  • [37] Crystal structure of (5S,4R)-5-(2-oxo-2-phenylethyl)-4-(phenylsulfanyl)2(3H)-dihydrofuranone, C18H16O3S
    Spek, AL
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 1997, 212 (02): : 257 - 258
  • [38] Synthesis and studies on the crystal structure of (2S,4R)-2-bromomethyl-2(2,4-dichlorophenyl)-1,3-dioxolan-4-methyl benzoate
    Qiu, YY
    Li, QL
    Yao, TW
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2004, 23 (06) : 712 - 716
  • [39] Efficient and practical asymmetric synthesis of 1-tert-butyl 3-methyl (3R,4R)-4-(2-oxo-2,3-dihydro-1H-benzimidazol-1-yl)piperidine-1,3-dicarboxylate, a useful intermediate for the synthesis of nociceptin antagonists
    Jona, Hideki
    Shibata, Jun
    Asai, Masanori
    Goto, Yasuhiro
    Arai, Sachie
    Nakajima, Shigeru
    Okamoto, Osamu
    Kawamoto, Hiroshi
    Iwasawa, Yoshikazu
    TETRAHEDRON-ASYMMETRY, 2009, 20 (21) : 2439 - 2446
  • [40] Crystal structure of cis-4-tert-butyl-2-(4-nitrophenylsulfonyl)cyclohexanone, C16H21NO5S
    Zukerman-Schpector, J.
    Maganhi, S.
    Olivato, P. R.
    Vinhato, E.
    Cerqueira, C. R., Jr.
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2006, 221 (02): : 165 - 166