Complete H-1 and C-13 NMR assignments of the oligosaccharide antibiotic Sch 27899

被引：0
|
作者：
Chan, TM
Osterman, RM
Morton, JB
Ganguly, AK
机构：
来源：
MAGNETIC RESONANCE IN CHEMISTRY | 1997年 / 35卷 / 08期
关键词：
NMR; H-1; C-13; HMQC; HMQC-TOCSY; HMBC; everninomicin;
D O I：
10.1002/(SICI)1097-458X(199708)35:8<529::AID-OMR120>3.0.CO;2-7
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The complete assignments of H-1 and C-13 data for Sch 27899 are described. The compound is an oligosaccharide antibiotic belonging to the class everninomicin. It has a molecular mass of 1629. The assignments are based on 2D HMQC, HMQC-TOCSY and HMBC experiments. (C) 1997 by John Wiley & Sons, Ltd.
引用
收藏
页码：529 / 532
页数：4
相关论文
共 50 条
  • [41] COMPLETE H-1 AND C-13 NMR ASSIGNMENTS OF TALLYSOMYCIN S10B BY MODERN 2-DIMENSIONAL NMR TECHNIQUES
    FREYDER, CP
    MARZILLI, LG
    [J]. MAGNETIC RESONANCE IN CHEMISTRY, 1991, 29 (04) : 338 - 350
  • [42] COMPLETE ASSIGNMENT OF THE H-1 AND C-13 NMR-SPECTRA AND SOLUTION CONFORMATION OF THE ANTITUMOR ANTIBIOTIC, ACLACINOMYCIN-A
    PARKINSON, JA
    SADLER, IH
    PICKUP, MB
    TABOR, AB
    [J]. TETRAHEDRON, 1995, 51 (26) : 7215 - 7222
  • [43] COMPLETE ASSIGNMENT OF THE H-1 AND C-13 NMR-SPECTRA OF NORBORNENE DERIVATIVES
    FISHER, J
    GRADWELL, MJ
    [J]. MAGNETIC RESONANCE IN CHEMISTRY, 1991, 29 (10) : 1068 - 1069
  • [44] COMPLETE ASSIGNMENT OF THE H-1 AND C-13 NMR-SPECTRA OF DEOXYHEMIGOSSYPOL DERIVATIVES
    ALAM, TM
    ROSAY, M
    DECK, L
    ROYER, R
    [J]. MAGNETIC RESONANCE IN CHEMISTRY, 1994, 32 (09) : 561 - 563
  • [45] Complete H-1 and C-13 NMR analysis of an asymmetric Troger's base
    Pardo, C
    Ramos, M
    Fruchier, A
    Elguero, J
    [J]. MAGNETIC RESONANCE IN CHEMISTRY, 1996, 34 (09) : 708 - 710
  • [46] H-1 AND C-13 CHEMICAL-SHIFT ASSIGNMENTS OF HOMOISOFLAVANONES
    ADINOLFI, M
    LANZETTA, R
    LAONIGRO, G
    PARRILLI, M
    BREITMAIER, E
    [J]. MAGNETIC RESONANCE IN CHEMISTRY, 1986, 24 (08) : 663 - 666
  • [47] SOLASODINE AND DIOSGENIN - H-1 AND C-13 ASSIGNMENTS BY 2-DIMENSIONAL NMR-SPECTROSCOPY
    PURI, R
    WONG, TC
    PURI, RK
    [J]. MAGNETIC RESONANCE IN CHEMISTRY, 1993, 31 (03) : 278 - 282
  • [48] H-1 and C-13 NMR assignments for 3- and 8-episirohydrochlorin methyl esters
    Burkhalter, RS
    Timkovich, R
    [J]. MAGNETIC RESONANCE IN CHEMISTRY, 1997, 35 (09) : 650 - 652
  • [49] SEQUENTIAL H-1, C-13, AND N-15 NMR ASSIGNMENTS AND SOLUTION CONFORMATION OF APOKEDARCIDIN
    CONSTANTINE, KL
    COLSON, KL
    WITTEKIND, M
    FRIEDRICHS, MS
    ZEIN, N
    TUTTLE, J
    LANGLEY, DR
    LEET, JE
    SCHROEDER, DR
    LAM, KS
    FARMER, BT
    METZLER, WJ
    BRUCCOLERI, RE
    MUELLER, L
    [J]. BIOCHEMISTRY, 1994, 33 (38) : 11438 - 11452
  • [50] BIOSYNTHETIC-STUDIES ON VALIDAMYCINS .1. H-1 AND C-13 NMR ASSIGNMENTS OF VALIDAMYCIN-A
    JIN, WZ
    RINEHART, KL
    TOYOKUNI, T
    [J]. JOURNAL OF ANTIBIOTICS, 1987, 40 (03): : 329 - 339
12345