Preparation and spectroscopic properties of some new diaroylmethanatoboron difluoride derivatives

被引：20

作者：

Wang, Dun-Jia ^{[1
]}

Xu, Ben-Po ^{[1
]}

Wei, Xian-Hong ^{[1
]}

Zheng, Jing ^{[1
]}

机构：

[1] Hubei Normal Univ, Hubei Key Lab Pollutant & Reuse Technol, Coll Chem & Environm Engn, Huangshi 435002, Peoples R China

来源：

JOURNAL OF FLUORINE CHEMISTRY | 2012年 / 140卷

关键词：

Diaroylmethanatoboron difluoride; Preparation; Diaroylmethanes; Spectroscopic properties; BORON DIFLUORIDE; CRYSTAL-STRUCTURE; LUMINESCENCE;

D O I：

10.1016/j.jfluchem.2012.04.010

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Five diaroylmethanatoboron difluoride derivatives were prepared from aryl methyl ketones via Claisen condensation with aromatic esters and followed by complexation with boron trifluoride etherate. Their structures and spectroscopic properties were studied by elemental analysis, IR, NMR, ESI-MS, UV and fluorescence spectroscopy. The results showed that these boron complexes had strong fluorescent peaks in the 400-500 nm range in chloroform and high quantum yields. The emission peaks for boron complexes containing naphthyl group exhibited considerable red shift as compared to those of containing phenyl group. (C) 2012 Elsevier B.V. All rights reserved.

引用

页码：49 / 53

页数：5

共 50 条

[1] PREPARATION AND SOME PROPERTIES OF GERMANIUM DIFLUORIDE
BARTLETT, N
YU, KC
CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1961, 39 (01): : 80 - &
[2] The preparation and properties of some new derivatives of pyridine
LaForge, FB
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1928, 50 : 2477 - 2483
[3] The preparation and properties of some new furan derivatives
Peters, FN
Fischer, R
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1930, 52 : 2079 - 2082
[4] Preparation and Properties of Some New Pyrazole Derivatives
Tinmaz, Feyza
Ilhan, Ilhan Ozer
Akkoc, Senem
ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 2020, 53 (01) : 89 - 94
[5] PREPARATION AND SPECTROSCOPIC PROPERTIES OF SOME NEW ASYMMETRIC ORGANOSILANES
HOLT, A
JARVIE, AWP
JERVIS, GJ
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1973, (02): : 114 - 122
[6] Spectroscopic Properties and Preparation of Some 2,3-Dimethoxybenzamide Derivatives
Cakmak, Sukriye
Kutuk, Halil
Odabasoglu, Mustafa
Yakan, Hasan
Buyukgungor, Orhan
LETTERS IN ORGANIC CHEMISTRY, 2016, 13 (03) : 181 - 194
[7] PREPARATION AND SPECTROSCOPIC PROPERTIES OF SOME MOLYBDENUM CARBONYL DERIVATIVES OF AMMONIA AND PHOSPHINE
BARLOW, CG
HOLYWELL, GC
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1969, 16 (03) : 439 - +
[8] PREPARATION AND PROPERTIES OF SOME NEW DERIVATIVES OF SILANE AND DISILANE
MACDIARMID, AG
ABEDINI, M
STERNBACH, B
CRAIG, AD
URENOVITCH, JV
WARD, LGL
SCIENCE, 1960, 132 (3438) : 1495 - 1496
[9] THE PREPARATION AND SPECTRAL PROPERTIES OF SOME NEW DERIVATIVES OF ACETOPHENONETRICARBONYLCHROMIUM
ARMSTRONG, BM
BOWEN, ME
CLARK, ML
FOLEY, BL
HAMILTON, JB
MAHAFFY, CAL
RAWLINGS, J
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1989, 197 : 455 - INOR
[10] Preparation and properties of some new extended tetrathiafulvalene (TTF) derivatives
Faldt, A
Pedersen, MJ
Krogh, TP
Hviid, L
Christensen, JB
SYNTHETIC METALS, 1998, 94 (03) : 307 - 310

← 1 2 3 4 5 →