Efficient one-pot room-temperature synthesis of 2-imidazolines from aldehydes

被引:0
|
作者
Alinezhad, H. [1 ]
Nemati, K. [1 ]
Zare, M. [2 ]
机构
[1] Univ Mazandaran, Dept Organ Chem, Fac Chem, Babol Sar, Iran
[2] Amol Univ Special Modern Technol, Fac Herbs, Dept Basic Sci, Amol, Iran
来源
BULGARIAN CHEMICAL COMMUNICATIONS | 2015年 / 47卷 / 03期
关键词
Imidazoline; Aldehyde; Ethylenediamine; N-Iodosaccharin; SOLVENT-FREE SYNTHESIS; BENZIMIDAZOLES; OXIDATION; 2-ARYLIMIDAZOLINES; IMIDAZOLINES; NITRILES; ALCOHOLS; MILD;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The reactions of various aromatic and aliphatic aldehydes with ethylenediamine followed by N-iodosaccharin treatment proceed at room temperature to give the corresponding dihydroimidazoles in high yields. The process is simple, fast and convenient.
引用
收藏
页码:804 / 808
页数:5
相关论文
共 50 条
  • [1] Diastereoselective One-Pot Synthesis of Tetrafunctionalized 2-Imidazolines
    Janssen, Guido V.
    Slobbe, Paul
    Mooijman, Maurice
    Kruithof, Art
    Ehlers, Andreas W.
    Guerra, Celia Fonseca
    Bickelhaupt, F. Matthias
    Slootweg, J. Chris
    Ruijter, Eelco
    Lammertsma, Koop
    Orru, Romano V. A.
    [J]. JOURNAL OF ORGANIC CHEMISTRY, 2014, 79 (11): : 5219 - 5226
  • [2] Mild and efficient one-pot synthesis of 2-imidazolines from nitriles using sodium hydrosulfide as catalyst
    Sun, Min
    Wei, Hong-Tao
    Li, Dong
    Zheng, You-Guang
    Cai, Jin
    Ji, Min
    [J]. SYNTHETIC COMMUNICATIONS, 2008, 38 (18) : 3151 - 3158
  • [3] One-Pot Synthesis of 2-Imidazolines via the Ring Expansion of Imidoyl Chlorides with Aziridines
    Kuszpit, Michael R.
    Wulff, William D.
    Tepe, Jetze J.
    [J]. JOURNAL OF ORGANIC CHEMISTRY, 2011, 76 (08): : 2913 - 2919
  • [4] Efficient and One-Pot Catalytic Synthesis of 2-Imidazolines and Bis-Imidazolines with p-Toluenesulfonic Acid under Solvent Free Conditions
    Nasr-Esfahani, Masoud
    Montazerozohori, Morteza
    Mehrizi, Safie
    [J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 2011, 48 (02) : 249 - 254
  • [5] Synthesis of aldehydes from carboxylic acids via 2-imidazolines
    Shi, Z
    Gu, H
    [J]. SYNTHETIC COMMUNICATIONS, 1997, 27 (15) : 2701 - 2707
  • [6] One-pot synthesis of imidazolines from aldehydes: detailed study about solvents and substrates
    Fujioka, Hiromichi
    Murai, Kenichi
    Kubo, Ozora
    Ohba, Yusuke
    Kita, Yasuyuki
    [J]. TETRAHEDRON, 2007, 63 (03) : 638 - 643
  • [7] Efficient one-pot synthesis of dihydroquinolinones in water at room temperature
    Linsenmeier, Anna M.
    Braje, Wilfried M.
    [J]. TETRAHEDRON, 2015, 71 (38) : 6913 - 6919
  • [8] An Overview of the One-pot Synthesis of Imidazolines
    Aneeja, Thaipparambil
    Radhika, Sankaran
    Neetha, Mohan
    Anilkumar, Gopinathan
    [J]. CURRENT ORGANIC CHEMISTRY, 2020, 24 (20) : 2341 - 2355
  • [9] A mild and efficient one-pot synthesis of 2-dihydroimidazoles from aldehydes
    Fujioka, H
    Murai, K
    Ohba, Y
    Hiramatsu, A
    Kita, Y
    [J]. TETRAHEDRON LETTERS, 2005, 46 (13) : 2197 - 2199
  • [10] A Facile and Efficient Synthesis of 2-Imidazolines from Aldehydes Using Hydrogen Peroxide and Substoichiometric Sodium Iodide
    Bai, Guo-yi
    Xu, Kai
    Chen, Guo-feng
    Yang, Yong-hui
    Li, Tian-yu
    [J]. SYNTHESIS-STUTTGART, 2011, (10): : 1599 - 1603