Software support for the Nordtest method of measurement uncertainty evaluation

被引:10
|
作者
Naykki, Teemu [1 ]
Virtanen, Atte [2 ]
Leito, Ivo [3 ]
机构
[1] Finnish Environm Inst, Environm Measurement & Testing Lab, Helsinki 00430, Finland
[2] Finnish Environm Inst, Data & Informat Ctr, Helsinki 00251, Finland
[3] Univ Tartu, Inst Chem, EE-50411 Tartu, Estonia
关键词
Measurement uncertainty; Validation; Within-laboratory reproducibility; Bias; Software; Testing laboratories; Quality control; Proficiency testing; Nordtest;
D O I
10.1007/s00769-012-0932-0
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Software support for the Nordtest method of measurement uncertainty evaluation is described. According to the Nordtest approach, the combined measurement uncertainty is broken down into two main components-the within-laboratory reproducibility (intermediate precision) s (Rw) and the uncertainty due to possible laboratory bias u(bias). Both of these can be conveniently estimated from validation and quality control data, thus significantly reducing the need for performing dedicated experiments for estimating detailed uncertainty contributions and thereby making uncertainty estimation easier for routine laboratories. An additional merit of this uncertainty estimation approach is that it reduces the danger of underestimating the uncertainty, which continues to be a problem at routine laboratories. The described software tool-MUkit (measurement uncertainty kit)-fully reflects the versatility of the Nordtest approach: it enables estimating the uncertainty components from different types of data, and the data can be imported using a variety of means such as different laboratory data systems and a dedicated web service as well as manual input. Prior to the development of the MUkit software, a laboratory survey was carried out to identify the needs of laboratories related to uncertainty estimation and other quality assurance procedures, as well as their needs for a practical tool for the calculation of measurement uncertainty.
引用
收藏
页码:603 / 612
页数:10
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