Quantitative Analysis of Sodium Carbonate and Sodium Bicarbonate in Solid Mixtures Using Fourier Transform Infrared Spectroscopy (FT-IR)

被引：64
|
作者：
Joshi, Shailesh [1 ]
Kalyanasundaram, Sivasubramanian [1 ]
Balasubramanian, Venkatraman [1 ]
机构：
[1] Indira Gandhi Ctr Atom Res, Radiol Safety Div, Kalpakkam 603102, Tamil Nadu, India
来源：
APPLIED SPECTROSCOPY | 2013年 / 67卷 / 08期
关键词：
Fourier transform infrared spectroscopy; FT-IR; Constant ratio method; Absorbance correction method; Sodium carbonate; Sodium bicarbonate; Internal standard; Liquid metal-cooled fast breeder reactors (LMFBR); CONSTANT RATIO METHOD; QUANTIFICATION; AEROSOL; ATMOSPHERE; SPECIATION; SAMPLES; BLENDS; WATER; FIRE;
D O I：
10.1366/12-06915
中图分类号：
TH7 [仪器、仪表];
学科分类号：
0804 ; 080401 ; 081102 ;
摘要：
An analytical methodology is proposed based on constant ratio and absorbance correction methods to quantify sodium carbonate, Na2CO3 (1450 cm(-1)), and sodium bicarbonate, NaHCO3 (1000 cm(-1), 1923 cm(-1)), in solid mixtures using Fourier transform infrared (FT-IR) spectroscopy. Potassium ferricyanide, K3Fe(CN)(6) (2117cm(-1)), was used as an internal standard to get characteristic parameters. NaHCO3 was quantified using the constant ratio method. Spectral interference of NaHCO3 in Na2CO3 (1450 cm(-1)) was corrected using the absorbance correction method. The corrected absorbance was successfully applied to quantify Na2CO3 (1450 cm(-1)) in the mixture using the constant ratio method. The results obtained for simulated samples were satisfactory (relative standard deviation less than 7%) for all samples.
引用
收藏
页码：841 / 845
页数：5
相关论文
共 50 条
  • [41] A novel direct coupling of simultaneous thermal analysis (STA) and Fourier transform-infrared (FT-IR) spectroscopy
    A. Schindler
    G. Neumann
    A. Rager
    E. Füglein
    J. Blumm
    T. Denner
    [J]. Journal of Thermal Analysis and Calorimetry, 2013, 113 : 1091 - 1102
  • [42] Fourier-transform infrared (FT-IR) spectroscopy analysis discriminates asymptomatic and symptomatic Norway spruce trees
    Mukrimin, Mukrimin
    Conrad, Anna O.
    Kovalchuk, Andriy
    Julkunen-Tiitto, Riitta
    Bonello, Pierluigi
    Asiegbu, Fred O.
    [J]. PLANT SCIENCE, 2019, 289
  • [43] Developing a phenotyping tool for disease resistance in trees using Fourier transform infrared (FT-IR) and Raman spectroscopy
    Conrad, A. O.
    Sniezko, R. A.
    Rodriguez-Saona, L.
    Bonello, P.
    [J]. PHYTOPATHOLOGY, 2018, 108 (10)
  • [44] Identification and characterization of Salmonella serotypes using DNA spectral characteristics by Fourier Transform Infrared (FT-IR) spectroscopy
    Sundaram, Jaya
    Park, Bosoon
    Hinton, Arthur
    Yoon, Seung Chul
    Lawrence, Kurt C.
    [J]. SENSING FOR AGRICULTURE AND FOOD QUALITY AND SAFETY IV, 2012, 8369
  • [45] Fourier transform infrared (FT-IR) spectroscopy in bacteriology: towards a reference method for bacteria discrimination
    Ornella Preisner
    João Almeida Lopes
    Raquel Guiomar
    Jorge Machado
    José C. Menezes
    [J]. Analytical and Bioanalytical Chemistry, 2007, 387 : 1739 - 1748
  • [46] Identification of coryneform bacteria and related taxa by Fourier-transform infrared (FT-IR) spectroscopy
    Oberreuter, H
    Seiler, H
    Scherer, S
    [J]. INTERNATIONAL JOURNAL OF SYSTEMATIC AND EVOLUTIONARY MICROBIOLOGY, 2002, 52 : 91 - 100
  • [47] Characterization of Large Amyloid Fibers and Tapes with Fourier Transform Infrared (FT-IR) and Raman Spectroscopy
    Ridgley, Devin M.
    Claunch, Elizabeth C.
    Barone, Justin R.
    [J]. APPLIED SPECTROSCOPY, 2013, 67 (12) : 1417 - 1426
  • [48] THE DETERMINATION OF DIFFUSION-COEFFICIENTS IN SEMISOLIDS BY FOURIER-TRANSFORM INFRARED (FT-IR) SPECTROSCOPY
    WURSTER, DE
    BURAPHACHEEP, V
    PATEL, JM
    [J]. PHARMACEUTICAL RESEARCH, 1993, 10 (04) : 616 - 620
  • [49] Application of Fourier transform infrared (FT-IR) spectroscopy and multivariate analysis for detection of adulteration in honey markets in Ethiopia
    Damto, Teferi
    Zewdu, Ashagrie
    Birhanu, Tarekegn
    [J]. CURRENT RESEARCH IN FOOD SCIENCE, 2023, 7
  • [50] Fourier transform infrared (FT-IR) spectroscopy in bacteriology: towards a reference method for bacteria discrimination
    Preisner, Ornella
    Lopes, Joao Almeida
    Guiomar, Raquel
    Machado, Jorge
    Menezes, Jose C.
    [J]. ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2007, 387 (05) : 1739 - 1748
12345