A facile two-step synthesis of 1,3,5-trinitrobenzene

被引：7
|
作者：
Bottaro, JC [1 ]
Malhotra, R [1 ]
Dodge, A [1 ]
机构：
[1] SRI Int, Chem Sci & Technol Lab, Menlo Pk, CA 94025 USA
来源：
SYNTHESIS-STUTTGART | 2004年 / 04期
关键词：
1,3,5-trintirobenzene; cyclohexanetrione trioximes; phloroglucinol;
D O I：
10.1055/s-2004-815958
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Synthesis of 1,3,5-trinitrobenzene was achieved by converting phloroglucinol into its trioximes by reaction with aqueous hydroxylamine followed by oxidation of the trioxime product with 90% nitric acid.
引用
收藏
页码：499 / 500
页数：2
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