Spectroscopic and Thermogravimetric Characterization of Pb(II) Dinonyldithiophosphate: Removal of Pb(II) from Aqueous Solution

被引：0
|
作者：
Gumgum, H. B. [1 ]
Biricik, N. [1 ]
机构：
[1] Dicle Univ, TR-21280 Diyarbakir, Turkey
来源：
JOURNAL OF APPLIED SPECTROSCOPY | 2015年 / 82卷 / 03期
关键词：
dinonyldithiophosphate; extraction; removal of lead; spectroscopy; thermogravimetric analysis; ORGANOPHOSPHORUS PESTICIDES; TRANSFORMATION PRODUCTS; METAL-COMPLEXES; CYANEX; 302; EXTRACTION; DITHIOPHOSPHATE; ANTIWEAR; LEAD(II); WATER; ACIDS;
D O I：
10.1007/s10812-015-0133-9
中图分类号：
O433 [光谱学];
学科分类号：
0703 ; 070302 ;
摘要：
Dinonyldithiophosphoric acid (DNDTPA) was prepared by adding phosphorus pentasulfide to nonyl alcohol. The lead dinonyl dithiophosphate complex Pb(DNDTP) (2) was prepared by mixing a solution of lead(II) with a solution of DNDTPA in ethanol at room temperature. The recovered Pb(DNDTP) (2) was crystallized in ethanol, and fi ne colorless needles were obtained. The complex was characterised by elemental analysis and IR, UV-vis and atomic absorption spectroscopy. The thermal behavior of Pb(DNDTP) (2) was investigated by thermogravimetric analysis under a nitrogen atmosphere. Removal of Pb(II) from aqueous media by DNDTPA solutions was investigated. The optimum conditions for extraction, such as the organic solvent, pH of the aqueous phase, time of equilibration, concentration, and effect of anions, were investigated. It was found that DNDTPA is an effective substance for removing Pb(II) from aqueous solution.
引用
收藏
页码：475 / 478
页数：4
相关论文
共 50 条
  • [41] Removal of Pb(II) from Aqueous Solution and Adsorption Kinetics of Corn Stalk Biochar
    Yang, Wenling
    Lu, Chaoyang
    Liang, Bo
    Yin, Chaohui
    Lei, Gao
    Wang, Baitao
    Zhou, Xiaokai
    Zhen, Jing
    Quan, Shujing
    Jing, Yanyan
    SEPARATIONS, 2023, 10 (08)
  • [42] Utilization of palm leaves as an extraordinary adsorbent for the removal of Pb(II) from an aqueous solution
    Almanassra, Ismail W.
    Khan, Muhammad Imran
    Chatla, Anjaneyulu
    Atieh, Muataz Ali
    Shanableh, Abdallah
    DESALINATION AND WATER TREATMENT, 2022, 271 : 206 - 219
  • [43] Removal of Pb(II) from aqueous solution using modified and unmodified kaolinite clay
    Jiang, Ming-qin
    Wang, Qing-ping
    Jin, Xiao-ying
    Chen, Zu-liang
    JOURNAL OF HAZARDOUS MATERIALS, 2009, 170 (01) : 332 - 339
  • [44] Ponkan peel: A potential biosorbent for removal of Pb(II) ions from aqueous solution
    Pavan, Flavio A.
    Mazzocato, Ana C.
    Jacques, Rosangela A.
    Dias, Silvio L. P.
    BIOCHEMICAL ENGINEERING JOURNAL, 2008, 40 (02) : 357 - 362
  • [45] Magnetic carboxylated cellulose nanocrystals as adsorbent for the removal of Pb(II) from aqueous solution
    Lu, Jiao
    Jin, Ru-Na
    Liu, Chao
    Wang, Yan-Fei
    Ouyang, Xiao-kun
    INTERNATIONAL JOURNAL OF BIOLOGICAL MACROMOLECULES, 2016, 93 : 547 - 556
  • [46] Removal of Pb (II) from aqueous solution by sulfur-functionalized walnut shell
    Xiu-guo Lu
    Yi-ting Guo
    Environmental Science and Pollution Research, 2019, 26 : 12776 - 12787
  • [47] Removal of Pb(II) ions from aqueous solution using complexation-ultrafiltration
    Sahin, Deniz
    Tascioglu, Senay
    POLISH JOURNAL OF CHEMICAL TECHNOLOGY, 2018, 20 (02) : 80 - 84
  • [48] Pb(II) and Cd(II) removal from aqueous solutions by olive cake
    Doyurum, Sabriye
    Celik, Ali
    JOURNAL OF HAZARDOUS MATERIALS, 2006, 138 (01) : 22 - 28
  • [49] REMOVAL OF Pb(II) FROM AQUEOUS SOLUTION BY CERAMSITE PREPARED FROM ISFAHAN BENTONITE AND γ-ALUMINA
    Mobasherpour, Iman
    Javaherai, Masomeh
    Salahi, Esmail
    Ebrahimi, Mohsen
    Ashrafi, Zahra
    Orooji, Yasin
    CHEMISTRY & CHEMICAL TECHNOLOGY, 2021, 15 (02): : 263 - 273
  • [50] Pb (II) REMOVAL FROM AQUEOUS SOLUTION BY ADSORPTION ON ACTIVATED CARBON FROM KIWI PEEL
    Rahimnejad, Mostafa
    Pirzadeh, Kasra
    Mahdavi, Iman
    Peyghambarzadeh, Seyed Mohsen
    ENVIRONMENTAL ENGINEERING AND MANAGEMENT JOURNAL, 2018, 17 (06): : 1293 - 1300
12345