Triterpene saponins from the roots of Bupleurum spinosum Gouan

被引：2

作者：

Dahmoune, Amina ^{[1
,2
]}

Smati, Dalila ^{[3
]}

Mitaine-Offer, Anne-Claire ^{[1
]}

Miyamoto, Tomofumi ^{[4
]}

Tanaka, Chiaki ^{[4
]}

Paululat, Thomas ^{[5
]}

Lacaille-Dubois, Marie-Aleth ^{[1
]}

机构：

[1] Univ Bourgogne Franche Comte, Lab Pharmacognosie, PEPITE EA 4267, UFR Sci Sante, BP 87900, F-21079 Dijon, France

[2] Univ Mouloud Mammeri, Fac Med, Tizi Ouzou, Algeria

[3] Univ Alger, Fac Med, Dept Pharm, Algiers, Algeria

[4] Kyushu Univ, Grad Sch Pharmaceut Sci, Fukuoka 8128582, Japan

[5] Univ Siegen, Organ Chem 2, Nat Wissensch Tech Fak, D-57076 Siegen, Germany

来源：

PHYTOCHEMISTRY LETTERS | 2020年 / 39卷

关键词：

Bupleurum spinosum; Apiaceae; Triterpene saponins; NMR spectroscopy; SAIKOSAPONINS;

D O I：

10.1016/j.phytol.2020.08.007

中图分类号：

Q94 [植物学];

学科分类号：

071001 ;

摘要：

Three previously undescribed triterpene saponins, and four known ones, were isolated from the EtOH/H2O extract of the roots of Bupleurum spinosum. Their structures were characterized using spectroscopic techniques including 1D and 2D NMR (H-1, C-13, COSY, TOCSY, ROESY, HSQC, and HMBC) experiments and mass spectrometry as 3-O-beta-D-glucopyranosyl-(1 -> 6)-[beta-D-glucopyranosyl-(1 -> 2)]-[alpha-L-rhamnopyranosyl-(1 -> 4)]-beta-D-glucopyranosyl-3 beta,16 beta,23,28-tetrahydroxyolean-12-ene, 3-O-beta-D-glucopyranosyl-(1 -> 6)-[beta-D-glucopyranosyl-(1 -> 2)]-[alpha-L-rhamnopyranosyl-(1 -> 4)]-beta-D-glucopyranosyl-3 beta,16 beta,28-trihydroxy-23-oxoolean-12-ene, 3-O-beta-D-glucopyranosyl-(1 -> 6)-[alpha-L-rhamnopyranosyl(1 -> 4)]-beta-D-glucopyranosyl-3 beta,16 beta,28-trihydroxyolean-12-ene-23-oic-acid. The chemotaxonomic significance is underlined.

引用

页码：157 / 161

页数：5

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