Molecular structures of methyl 4-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-1-methyl-1H-pyrazol-5-carboxylate and methyl 4-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-1-methyl-1H-pyrazol-3-carboxylate

被引：5

作者：

Sakhautdinov, I. M. ^{[1
]}

Batyrshin, I. R. ^{[1
]}

Fatykhov, A. A. ^{[1
]}

Yumabaeva, V. M. ^{[2
]}

Suponitskii, K. Yu. ^{[3
]}

Antipin, M. Yu. ^{[3
]}

Yunusov, M. S. ^{[1
]}

机构：

[1] Russian Acad Sci, Inst Organ Chem, Ufa Sci Ctr, Ufa 450001, Russia

[2] Bashkir State Univ, Ufa 450074, Russia

[3] Russian Acad Sci, AN Nesmeyanov Organoelement Cpds Inst, Moscow 117901, Russia

来源：

JOURNAL OF STRUCTURAL CHEMISTRY | 2013年 / 54卷 / 02期

关键词：

methyl 4-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-1-methyl-1H-pyrazol-5-carboxylate; methyl 4-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-1-methyl-1H-pyrazol-3-carboxylate; NMR spectroscopy; X-ray crystallography;

D O I：

10.1134/S0022476613020169

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The structure of methyl 4-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-1-methyl-1H-pyrazol-5-carboxylate is determined by X-ray crystallography and further used to elucidate the structure of methyl 4-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]-1-methyl-1H-pyrazol-3-carboxylate, using the data of homo- and heteronuclear 2D NMR correlation spectroscopy.

引用

页码：383 / 387

页数：5

共 50 条

[21] Crystal structure of (S)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionic acid methyl ester, C8H4NO2[CH(CH3)COOCH3]
Peters, K
Peters, EM
Griesbeck, AG
Oelgemöller, M
Bartoschek, A
[J]. ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 1999, 214 (01): : 107 - 108
[22] Diethyl [(2-bromoanilino)(1,3-diphenyl-1H-pyrazol-4-yl)methyl]phosphonate
Suresh, G.
Sabari, V.
Nandakumar, A.
Perumal, P. T.
Aravindhan, S.
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1554 - +
[23] Diethyl [benzylamino(1,3-diphenyl-1H-pyrazol-4-yl)methyl]phosphonate
Jagadeesan, G.
Suresh, G.
Nandakumar, B.
Perumal, P. T.
Aravindhan, S.
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2376 - U650
[24] CRYSTAL AND MOLECULAR-STRUCTURE OF 2-(1,3-DIOXO-1,3-DIHYDRO-ISOINDOL-2-YL)-3-(4-METHYL-5-OXO-2,5-DIHYDRO-FURAN-2-YLOXY)-BUT-2-ENOIC ACID METHYL-ESTER, C18H15NO7
MOERS, FG
SMITS, JMM
BEURSKENS, PT
VANGAAL, A
NEFKENS, G
ZWANENBURG, B
[J]. JOURNAL OF CRYSTALLOGRAPHIC AND SPECTROSCOPIC RESEARCH, 1993, 23 (10): : 829 - 831
[25] 3-Methyl-1-(pyridin-2-yl)-4-(1-pyridin-2-yl-3-methyl-1H-pyrazol-5-yl)-2H-3-pyrazolin-5(1H)-one
Djerrari, B
Essassi, EM
Fifani, J
Pierrot, M
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2001, 57 : O1126 - O1127
[26] (E)-4-(2,3-Dihydro-1,3-benzothiazol-2-ylidene)-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one
Chakibe, Imane
Zerzouf, Abdelfettah
Essassi, El Mokhtar
Reichelt, Martin
Reuter, Hans
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1096 - U274
[27] 4-[Tris(1H-pyrazol-1-yl)methyl]phenol
Chen, Xiao-Yan
Yang, Xiaoping
Holliday, Bradley J.
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3045 - U1490
[28] 1-Allyl-4-(1,3-benzothiazol-2-yl)-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one
Chakib, Imane
Zerzouf, Abdelfettah
Zouihri, Hafid
Essassi, El Mokhtar
Ng, Seik Weng
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2842 - U416
[29] Stacking in 5-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propoxy]-3-methyl-1-phenyl-1H-pyrazole-4-carboxylic acid ethyl ester through C-H•••π, C-H•••O and C-H•••N networks
Tewari, Ashish Kumar
Srivastava, Priyanka
Puerta, Carmen
Valerga, Pedro
[J]. JOURNAL OF MOLECULAR STRUCTURE, 2009, 921 (1-3) : 251 - 254
[30] 4-[(1,3-Dioxoisoindolin-2-yl)methyl]benzenesulfonamide
Mague, Joel T.
Abdel-Aziz, Alaa A. -M.
El-Azab, Adel S.
EI-Sherbeny, Magda A.
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O291 - +

← 1 2 3 4 5 →