Orientation analysis of bulk YBCO from incomplete neutron diffraction data

被引:10
|
作者
Chateigner, D [1 ]
Wenk, HR [1 ]
Pernet, M [1 ]
机构
[1] CNRS,LAB CRISTALLOG,F-38042 GRENOBLE 09,FRANCE
关键词
D O I
10.1107/S0021889896008758
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Highly incomplete pore figures of a magnetic-field-aligned melt-textured superconducting sample of the Y-Ba-Cu-O system were measured by neutron diffraction. The orientation distribution of the main superconducting 123 and a minor 211 phase have been derived with the WIMV algorithm. The 123 phase is strongly textured with a (001) maximum around 22 times that of a random distribution (m.r.d.) and a texture index of 30. There are two orientation components present that have no apparent relationship with the applied magnetic field. The texture of the 211 phase is weak, with a maximum of 1.7 m.r.d. The textures of the two phases appear to be correlated.
引用
收藏
页码:43 / 48
页数:6
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