The synthesis of microporous and mesoporous titania with high specific surface area using sol-gel method and activated carbon templates

被引:19
|
作者
Loryuenyong, Vorrada [1 ,2 ]
Buasri, Achanai [1 ,2 ]
Srilachai, Chonticha [1 ]
Srimuang, Hathaichanok [1 ]
机构
[1] Silpakorn Univ, Dept Mat Sci & Engn, Fac Engn & Ind Technol, Nakhon Pathom 73000, Thailand
[2] Chulalongkorn Univ, Natl Ctr Excellence Petr Petrochem & Adv Mat, Bangkok 10330, Thailand
关键词
Nanocrystalline TiO2; Sol-gel process; Activated carbon; Template; Micropores; TIO2;
D O I
10.1016/j.matlet.2012.07.090
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this study, porous titania nanoparticles were synthesized by sal-gel template method, using titanium (IV) tetraisopropoxide as a starting precursor and isopropanol as a solvent. Different commercial activated carbons were used as templates at 10 wt% in titania sol. The templates were completely removed during the calcination in air at 500 degrees C for 3 h, forming porous titania. Nanocrystalline anatase titania with specific surface area as high as 700 m(2)/g was successfully obtained in this study. This specific surface area is one of the highest values reported in the literature under similar sol-gel conditions. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码:47 / 50
页数:4
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