Efficient synthesis of 1,8-dioxo-octahydroxanthenes catalyzed by β-cyclodextrin grafted with butyl sulfonic acid in aqueous media

被引：13

作者：

Gong, Kai ^{[1
]}

Wang, Hualan ^{[2
]}

Wang, Shuxin ^{[1
]}

Wang, Ying ^{[1
]}

Chen, Jinghua ^{[1
]}

机构：

[1] Jiangnan Univ, Sch Pharmaceut Sci, Wuxi 214122, Jiangsu, Peoples R China

[2] Hangzhou Normal Univ, Key Lab Organosilicon Chem & Mat Technol, Minist Educ, Hangzhou 311121, Zhejiang, Peoples R China

来源：

CHINESE JOURNAL OF CATALYSIS | 2015年 / 36卷 / 08期

基金：

中国国家自然科学基金;

关键词：

One-pot synthesis; Acidic catalyst; beta-Cyclodextrin bearing butyl sulfonic acid; 1,8-Dioxo-octahydroxanthenes; Aqueous media; ONE-POT SYNTHESIS; HETEROGENEOUS CATALYST; DERIVATIVES; WATER; PERFORMANCE; AGENTS; ROUTE; DYES;

D O I：

10.1016/S1872-2067(15)60888-9

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

beta-Cyclodextrin was functionalized with butyl sulfonic acid to give an efficient, eco-friendly catalyst for the synthesis of 1,8-dioxo-octahydroxanthenes via the one-pot condensation of aromatic aldehydes and active methylene carbonyl compounds in aqueous media. This new methodology offers several advantages such as excellent yields, short reaction time, a simple procedure and mild reaction conditions. Furthermore, the catalyst can be readily recovered and reused up to five times without a significant loss in its activity. (C) 2015, Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by Elsevier B.V. All rights reserved.

引用

页码：1249 / 1255

页数：7

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