Synthesis and characterization of a novel heat resistant epoxy resin based on N,N′-bis(5-hydroxy-1-naphthyl)pyromellitic diimide

被引：52
|
作者：
Ren, Hua [1 ]
Sun, Jianzhong [1 ]
Zhao, Qian [1 ]
Zhou, Qiyun [1 ]
Ling, Qincai [1 ]
机构：
[1] Zhejiang Univ, Dept Chem & Biochem Engn, State Key Lab Chem Engn, Hangzhou 310027, Peoples R China
来源：
POLYMER | 2008年 / 49卷 / 24期
关键词：
Epoxy resin; Heat resistant; Naphthol;
D O I：
10.1016/j.polymer.2008.09.047
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
A novel epoxy resin containing imide and naphthyl groups was synthesized, and characterized using NMR, NMR, FT-IR spectra and elemental analyses. The curing behavior was investigated with differential scanning calorimetry (DSC) using 4,4'-diaminodiphenylsulfone (DDS) as curing agent. The physical properties of the cured polymer were evaluated with dynamic thermal mechanical analysis (DMTA) and thermogravimetric analysis (TGA). The results showed that the cured polymer exhibited higher glass transition temperature (T-g) and better thermal stability compared with those commercial available heat resistant epoxy resins. (c) 2008 Elsevier Ltd. All rights reserved.
引用
收藏
页码：5249 / 5253
页数：5
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