3,5-Bis[1-acetyl-5-(4-chlorophenyl)-4,5-dihydro-1H-pyrazol-3-yl]-2,6-dimethylpyridine tetrahydrofuran solvate

被引:1
|
作者
Qian, Qun [1 ]
Zhang, Jun [1 ]
Zhang, Min [1 ]
He, Xiang [1 ]
Xia, Yiben [2 ]
机构
[1] Shanghai Univ, Dept Chem, Coll Sci, Shanghai 200444, Peoples R China
[2] Shanghai Univ, Sch Mat Sci & Engn, Shanghai 200072, Peoples R China
关键词
D O I
10.1107/S1600536808018497
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C29H27Cl2N5O2 center dot C4H8O, the polycyclic system is composed of three parts: one central pyridine ring substituted by two functionalized pyrazoline rings. The dihedral angles between the central pyridine plane and pyrazoline planes are 5.11 (1) and 13.99 (1) degrees, whereas the dihedral angles between each chlorophenyl plane and the attached pyrazoline planes are 88.65 (1) and 83.87 (1). Molecules are linked by intermolecular C-H center dot center dot center dot O hydrogen bonds, forming a three-dimensional network.
引用
收藏
页码:O1334 / U2551
页数:13
相关论文
共 50 条
  • [21] 6-[1-Acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazole-3-yl]-2(3H)-benzoxazolone
    Ivanova, Yordanka
    Todorova, Antonya
    Chanev, Christo
    Petrov, Ognyan
    MOLBANK, 2018, (04)
  • [22] 1-[3-(4-Chlorophenyl)-5-(4-methoxyphenyl)- 4,5-dihydro-1H-pyrazol-1-yl]-butan-1-one
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Samshuddin, S.
    Narayana, B.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O975 - +
  • [23] 4-{3,5-Bis[2,3,5,6-tetrafluoro-4-(piperazin-1-yl)phenyl]-4,5-dihydro-1H-pyrazol-1-yl}benzaldehyde in the Synthesis of New Dendritic Chromophores
    Ishchenko, R. A.
    Orlova, N. A.
    Shelkovnikov, V. V.
    Maksimov, A. M.
    Ryazanov, N. D.
    Berezhnaya, V. N.
    Chernonosov, A. A.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2025, 61 (01) : 184 - 189
  • [24] Synthesis, Anticonvulsant, and Molecular Docking Studies of (3,5-disubstituted-4,5-dihydro-1H-pyrazol-1-yl) (4-chlorophenyl) Methanone Derivatives
    Ray, Pushkar Kumar
    Salahuddin
    Mazumder, Avijit
    Kumar, Rajnish
    Ahsan, Mohamed Jawed
    Yar, Mohammad Shahar
    INDIAN JOURNAL OF PHARMACEUTICAL EDUCATION AND RESEARCH, 2023, 57 (01) : 202 - 209
  • [25] 1-{3-(4-Chlorophenyl)-5-[4-(propan-2-yl)phenyl]-4,5-dihydro-1H-pyrazol-1-yl}-butan-1-one
    Narayana, B.
    Salian, Vinutha V.
    Sarojini, Balladka K.
    Jasinski, Jerry P.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 0761 - +
  • [26] 3-(4-Chlorophenyl)-5-(thiophen-2-yl)-4,5-dihydro-1H-pyrazole-1-carbothioamide
    Fun, Hoong-Kun
    Suwunwong, Thitipone
    Chantrapromma, Suchada
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : O259 - U1464
  • [27] 1-{3-(4-Chlorophenyl)-5-[4-(propan-2yl)phenyl]-4,5-dihydro-1H-pyrazol- 1-yl}propan-1-one
    Narayana, B.
    Salian, Vinutha V.
    Sarojini, Balladka K.
    Jasinski, Jerry P.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 0763 - +
  • [28] 2-[3-(4-Chlorophenyl)-5-(4-fluorophenyl)-4,5-dihydro-1H-pyrazol-1-yl]-4-phenyl-1,3-thiazole
    Abdel-Wahab, Bakr F.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O576 - +
  • [29] 4-[5-(4-Chlorophenyl)-3-methyl-1H-pyrazol-1-yl]benzenesulfonamide
    Farrukh, Muhammad A.
    Mohamed, Shaaban K.
    Ahmed, Maqsood
    Marzouk, Adel A.
    El-Moghazy, Samir M.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O295 - +
  • [30] 3,5-Diphenyl-1-(quinolin-2-yl)-4,5-dihydro-1H-pyrazol-5-ol
    Bin Najib, Muhd. Hidayat
    Tan, Ai Ling
    Young, David J.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02310 - +