Syntheses, structures, and properties of the Co(II), Ni(II), and Cu(II) complexes with 5-carboxy- and 5-methoxycarbonylpyrazoles

被引：3
|
作者：
Shakirova, O. G. [1 ]
Lavrenova, L. G. [1 ,2 ]
Kuratieva, N. V. [1 ,2 ]
Naumov, D. Yu. [1 ]
Bogomyakov, A. S. [3 ]
Sheludyakova, L. A. [1 ]
Mikhailovskaya, T. F. [4 ]
Vasilevsky, S. F. [4 ]
机构：
[1] Russian Acad Sci, Nikolaev Inst Inorgan Chem, Siberian Branch, Novosibirsk 630090, Russia
[2] Novosibirsk State Univ, Novosibirsk 630090, Russia
[3] Russian Acad Sci, Siberian Branch, Int Tomog Ctr, Novosibirsk 630090, Russia
[4] Russian Acad Sci, Siberian Branch, Inst Chem Kinet & Combust, Novosibirsk 630090, Russia
来源：
RUSSIAN JOURNAL OF COORDINATION CHEMISTRY | 2012年 / 38卷 / 08期
关键词：
MAGNETIC-PROPERTIES; PYRAZOLES; DIMENSIONALITY; LIGAND; ACID;
D O I：
10.1134/S107032841207010X
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
New cobalt(II), nickel(II), and copper(II) complexes based on 5-methoxycarbonyl-3-me-thylpyrazole (MePzCOOMe), [Co(MePzCOOMe)(2)(H2O)(2)](NO3)(2) (I), [Ni(MePzCOOMe)(2)(H2O)(2)] (NO3)(2) (II), and [Cu(MePzCOO)(2)(H2O)] center dot 3H(2)O (III), were synthesized. The compounds were studied by X-ray diffraction analysis, IR spectroscopy, and static magnetic susceptibility. The molecular and crystal structures of complexes I and III were determined by X-ray structure analysis.
引用
收藏
页码：552 / 559
页数：8
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