Isolation of the lignan secoisolariciresinol diglucoside from flaxseed (Linum usitatissimum L.) by high-speed counter-current chromatography

被引：47
|
作者：
Degenhardt, A [1 ]
Habben, S [1 ]
Winterhalter, P [1 ]
机构：
[1] Tech Univ Carolo Wilhelmina Braunschweig, Inst Food Chem, DE-38106 Braunschweig, Germany
来源：
JOURNAL OF CHROMATOGRAPHY A | 2002年 / 943卷 / 02期
关键词：
Linum usitatissimum; counter-current chromatography; plant materials; secoisolariciresinol diglucoside; glucosides; lignans phytoestrogens; plant hormones;
D O I：
10.1016/S0021-9673(01)01467-4
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
High-speed counter-current chromatography was successfully used for the isolation and purification of secoisolariciresinol diglucoside, a bioactive lignan from flaxseed (Linum usitatissimum L.). The solvent system consisted of tert.-butylmethyl ether-n-butanol-acetonitrile-water (1:3:1:5). The purity and identity of the isolated compound was checked by high-performance liquid chromatography analysis in combination with mass spectrometry and NMR measurements. (C) 2002 Elsevier Science B.V. All rights reserved.
引用
收藏
页码：299 / 302
页数：4
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