Optical lever for monitoring of the magic angle

被引:6
|
作者
Mihaliuk, Eugene [1 ]
Gullion, Terry [1 ]
机构
[1] W Virginia Univ, Dept Chem, Morgantown, WV 26506 USA
基金
美国国家科学基金会;
关键词
MAS NMR; Magic angle setting; Probe; NUCLEAR-MAGNETIC-RESONANCE; SOLID-STATE NMR; PROBE;
D O I
10.1016/j.jmr.2012.08.007
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Setting the magic angle and accurately maintaining it over a full range of experimental conditions can be a frustrating experience. We present a simple optical device for immediate indication of the stator angle, free of mechanical uncertainties present in typical adjustment mechanisms. (C) 2012 Elsevier Inc. All rights reserved.
引用
收藏
页码:46 / 50
页数:5
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