Isolation of Volatiles in Honeysuckle by Multiple Approaches with Determination by Gas Chromatography-Mass Spectrometry (GC-MS) and Headspace Solid-Phase Microextraction-Gas Chromatography-Mass Spectrometry (HS-SPME/GC-MS)

被引：2
|
作者：
Ni, Lijun [1 ]
Lu, Qingmei [1 ]
Hou, Huanyao [1 ]
Zhang, Liguo [1 ]
Luan, Shaorong [1 ]
机构：
[1] East China Univ Sci & Technol, Sch Chem & Mol Engn, Shanghai, Peoples R China
来源：
ANALYTICAL LETTERS | 2023年 / 56卷 / 14期
关键词：
Headspace solid-phase microextraction-gas chromatography-mass spectrometry (HS-SPME; GC-MS); honeysuckle; volatile components; water extraction coupling rectification; water extraction coupling rectification and solvent extraction; ESSENTIAL OILS; AERIAL PARTS; CHEMICAL-COMPOSITIONS; EXTRACTION; HYDRODISTILLATION;
D O I：
10.1080/00032719.2023.2168687
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The volatile components of honeysuckle were determined using hydro-distillation (HD), water extraction coupling rectification (WER), and water extraction coupling rectification with solvent extraction (WER-SE). Gas chromatography-mass spectrometry (GC-MS) and headspace solid-phase microextraction-gas chromatography-mass spectrometry (HS-SPME/GC-MS) identified 127 compounds. There were 27 common compounds extracted by these methods. A heatmap of the 27 common compounds indicates that WER-SE and WER were complementary approaches. In addition, 59 compounds were detected for the first time in honeysuckle. The results of this study provide a reference for the determination of volatile components in plants.
引用
收藏
页码：2359 / 2370
页数：12
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