Eco-friendly high-rate formation of silver nanoparticles in agave inulin and its bactericidal effect against Escherichia coli

被引:0
|
作者
Sanchez-Vieyra, Maria Teresa [1 ]
Ojeda-Martinez, Miguel [1 ]
Oceguera-Contreras, Eden [2 ]
Rodriguez-Preciado, Sergio Yair [2 ]
Diaz-Zaragoza, Mariana [2 ]
Martinez-Zerega, Brenda Esmeralda [3 ]
Gonzalez-Solis, Jose Luis [3 ]
Oseguera-Galindo, David Omar [1 ]
机构
[1] Univ Guadalajara, Ctr Univ Valles, Dept Cs Nat & Exactas, Carretera Guadalajara Ameca Km 45-5, Ameca 46600, Jalisco, Mexico
[2] Univ Guadalajara, Ctr Univ Valles, Dept Cs Salud, Carretera Guadalajara Ameca Km 45-5, Ameca 46600, Jalisco, Mexico
[3] Univ Guadalajara, Ctr Univ Lagos, Lab Biofis & Ciencias Biomed, Lagos De Moreno 47460, Jalisco, Mexico
关键词
silver nanoparticles; green synthesis; agave inulin; absorbance; bactericidal effect; ANTIMICROBIAL ACTIVITY; EXTRACT; SIZE;
D O I
10.2478/msp-2023-0034
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A high rate of silver nanoparticle formation, effective against the Escherichia coli(E. coli) bacterium, was obtained for the first time by means of a simple, eco-friendly, and low-cost green method in a solution of agave inulin. The study was carried out using the traditional method, in which the effects of the concentration of agave inulin, AgNO3, temperature, and pH on the synthesis were analyzed by UV-Vis spectroscopy and transmission electron microscopy (TEM). Most of the nanoparticles produced were spherical with a size less than 10 nm. In a sample with 20 mg/mL of agave inulin, 1 mM of AgNO3, T=23(degrees)C,and pH=12, the highest percentage of Ag(+ )ions available in the solution were reduced for the formation of nanoparticles in less than 40 min, whereas a sample prepared with 60 mg/mL of agave inulin, 10 mM of AgNO3, T=23(degrees)C, pH=12, and a storage time of 40 min showed a significant bactericidal effect on the E. colistrain. Agave inulin is a good biological compound for the formation of small, spherical silver nanoparticles. A pH of 12 favors a higher production speed of the silver nanoparticles and better use of the available Ag(+ )ions. In addition to this, the concentration of AgNO(3)is a determining factor for increased formation of the nanoparticles necessary to bactericidal effect
引用
收藏
页码:62 / 73
页数:12
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