Deposition of boron coatings on surfaces by electron-beam evaporation in forevacuum

被引:1
|
作者
Yushkov, Yu. G. [1 ,2 ]
Meisner, S. N. [3 ]
Oks, E. M. [1 ,2 ]
Ostapenko, M. G. [3 ]
Tyunkov, A. V. [1 ]
Zolotukhin, D. B. [1 ]
机构
[1] Tomsk State Univ Control Syst & Radioelect, 40 Lenin Ave, Tomsk 634050, Russia
[2] Inst High Current Elect SB RAS, 2-3Akademichesky Ave, Tomsk 634055, Russia
[3] Inst Strength Phys & Mat Sci SB RAS, 2-4Pr Akad Sky, Tomsk 634055, Russia
基金
俄罗斯科学基金会;
关键词
Thin boron films; Electron-beam evaporation; Beam plasma; Forevacuum range of pressure;
D O I
10.1016/j.ceramint.2022.09.359
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
We implemented the boron coating deposition on the surface by means of electron-beam evaporation of a crystalline pure boron target (99.9%) and ionization of its vapor at a forevacuum pressure (5-15 Pa). The results of studying the characteristics of this process are presented. The space-angular distribution of the substrate temperature and the distribution of deposition rate for different temperatures of the evaporated target, which is determined by the distribution of boron particles in the volume of the vacuum chamber, were obtained. We give the results of measurements of the plasma composition for three stages of thermal processing of the pure boron target: heating, melting, and intense evaporation. Pure boron coatings on titanium samples at different tem-peratures were synthesized. The effect of the substrate temperature on the morphology and properties of boron coatings was investigated. It was found that boron in coatings is mostly in an amorphous state, while at the coating boundary it forms chemical compounds with titanium, phases of which were determined using X-ray diffraction pattern method. The results of our work may be useful for a wide range of applications that use thin boron films on various surfaces.
引用
收藏
页码:4701 / 4706
页数:6
相关论文
共 50 条
  • [41] On the possibility of electron-beam processing of dielectrics using a forevacuum plasma electron source
    Burdovitsin, V. A.
    Klimov, A. S.
    Oks, E. M.
    TECHNICAL PHYSICS LETTERS, 2009, 35 (06) : 511 - 513
  • [42] On the possibility of the electron-beam welding of quartz glasses by a forevacuum plasma electron source
    Zenin, A. A.
    Klimov, A. S.
    Oksa, E. M.
    CERAMICS INTERNATIONAL, 2019, 45 (04) : 4798 - 4801
  • [43] EVAPORATION OF METALS BY AN ELECTRON-BEAM OF AN ELECTRON MICROSCOPE
    SHIMAOKA, G
    VACUUM, 1965, 15 (09) : 452 - &
  • [44] ELECTRON-BEAM CURING OF COATINGS
    DUPLESSIS, TA
    DEHOLLAIN, G
    JOURNAL OF THE OIL & COLOUR CHEMISTS ASSOCIATION, 1979, 62 (07): : 239 - 245
  • [45] ELECTRON-BEAM CURING OF COATINGS
    TAWN, ARH
    JOURNAL OF THE OIL & COLOUR CHEMISTS ASSOCIATION, 1968, 51 (09): : 782 - &
  • [46] CERAMIC COATINGS VIA ELECTRON-BEAM PHYSICAL VAPOR-DEPOSITION
    BIANCHI, LM
    HALNAN, WK
    SHEN, S
    AMERICAN CERAMIC SOCIETY BULLETIN, 1981, 60 (03): : 393 - 393
  • [47] SIMULATION OF ELECTRON-BEAM EVAPORATION OF POLYMERS
    FAINSHTEIN, AI
    SILANTEV, AI
    VYSOKOMOLEKULYARNYE SOEDINENIYA SERIYA A, 1988, 30 (04): : 834 - 838
  • [48] Electron-beam deposition of polyethylene composite coatings at various initiators and inhibitors
    Liu, Zhubo
    Rogachev, A. A.
    Zhou, Bing
    Yarmolenko, M. A.
    Rogachev, A. V.
    Gorbachev, D. L.
    Jiang, Xiaohong
    POLYMER ENGINEERING AND SCIENCE, 2012, 52 (10): : 2134 - 2139
  • [49] FORMATION OF GRADIENT METALLOCERAMIC MATERIALS USING ELECTRON-BEAM IRRADIATION IN THE FOREVACUUM
    Klimov, A. S.
    Zenin, A. A.
    Bakeev, I. Yu.
    Oks, E. M.
    RUSSIAN PHYSICS JOURNAL, 2019, 62 (07) : 1123 - 1129
  • [50] EVAPORATION RATE DISTRIBUTION DURING ELECTRON-BEAM EVAPORATION
    TENCHOV, C
    SIMEONOVA, DS
    MITEV, VA
    DONKOV, N
    MEASUREMENT SCIENCE AND TECHNOLOGY, 1993, 4 (10) : 1050 - 1051