Design and performance evaluation of an all-ceramic high-temperature test sensor

被引:7
|
作者
Niu, Yanyan [1 ,2 ,3 ]
Dong, Helei [1 ,2 ,3 ]
Wang, Hanyu [1 ,2 ,3 ]
Liu, Tao [1 ,2 ,3 ]
Li, Xiangpeng [1 ,2 ,3 ]
Tan, Qiulin [1 ,2 ,3 ]
Xiong, Jijun [1 ,2 ,3 ]
机构
[1] North Univ China, Sch Instruments & Elect, Taiyuan 030051, Peoples R China
[2] North Univ China, State Key Lab Dynam Measurement Technol, Taiyuan 030051, Peoples R China
[3] North Univ China, Sci & Technol Elect Test & Measurement Lab, Taiyuan 030051, Peoples R China
基金
中国国家自然科学基金; 中国博士后科学基金;
关键词
Ceramic materials; Screen printing; Thick film thermocouple; Seebeck coefficient; High temperature test; THIN-FILM THERMOCOUPLES; MICROSTRUCTURE; FABRICATION; STABILITY; MECHANISM; OXIDES;
D O I
10.1016/j.jallcom.2022.168561
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
To meet the test requirements for the surface temperature parameters of next-generation ceramic matrix composite equipment components, this study designed and fabricated an all-ceramic material high-tem-perature test sensor, including a substrate, sensitive layer, and protective layer. The sensor was prepared using the thick-thin film integration process. The ITO-In2O3 thick film thermocouple was prepared on ceramic substrate using screen printing technology, and the Al2O3 thin film protective layer was prepared by pulsed laser ablation and the sol-gel method. Scanning electron microscopy (SEM), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS) were used to study the microstructure, phase, surface element composition and chemical transition state of the prepared thermocouple. The results show that the sintered thermocouple has a compact structure and good electrical conductivity. Static and dynamic test platforms were built to test the performance of thermocouple, and test results show that the prepared thermocouple has good repeatability and stability in the temperature range of 25-1300 degrees C. The average Seebeck coefficient reached 129.80 mu V/degrees C. In the thermoelectric stability evaluation experiment (1300 degrees C for 8 h), the peak output voltage was 153.2 mV. The limit test temperature of the thermocouple reached 1500 degrees C. When the temperature difference was 1382 degrees C, the peak output voltage was 169.974 mV. The dynamic properties of the sensor were studied using pulsed laser heating, and the results showed that the dynamic response time constant of the thermocouple was 3.52 ms.(c) 2022 Elsevier B.V. All rights reserved.
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页数:9
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