Explanation and prediction of the selective crystallization of boscalid by mid-frequency Raman difference spectroscopy analysis

被引：2
|
作者：
Fan, Yingjie [1 ,2 ]
Liang, Chengfeng [2 ]
Li, Yanping [2 ]
Xiao, Wangchuan [2 ]
Niu, Yu [2 ]
Jin, Hongjun [1 ]
Xue, Rongrong [2 ]
Chen, Fenghua [2 ]
机构：
[1] Fujian Normal Univ, Coll Environm & Resource Sci, Fuzhou 350007, Fujian, Peoples R China
[2] Sanming Univ, Sch Resources & Chem Engn, Sanming 365004, Fujian, Peoples R China
来源：
CRYSTENGCOMM | 2023年 / 25卷 / 24期
基金：
中国国家自然科学基金;
关键词：
CRYSTAL NUCLEATION; INSIGHT; INOSINE;
D O I：
10.1039/d2ce01679f
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The selective crystallization behaviours of amorphous boscalid (BOS), BOS monohydrate and acetone/ethyl acetate/ethanol/methanol solutions were explained and predicted by mid-frequency Raman difference spectroscopy analysis. The phase transition processes including solution to amorphous BOS, solution to BOS monohydrate, and amorphous BOS to Form I were explained, predicted and realized. Also, suitable preparation routes for different BOS phases with good purities were proposed.
引用
收藏
页码：3548 / 3555
页数：8
相关论文
共 50 条
  • [1] Explanation for the selective crystallization from inosine solutions using mid-frequency Raman difference spectra analysis
    Chen, Fenghua
    Yang, Chenmei
    Cheng, Xinyu
    Fan, Yingjie
    Chen, Xinyuan
    Ren, Shizhao
    Xue, Rongrong
    [J]. RSC ADVANCES, 2022, 12 (29) : 18301 - 18306
  • [2] Explanation and prediction for the product of trehalose dihydrate selective dehydration process using mid-frequency Raman difference spectra
    Fan, Yingjie
    Xue, Rongrong
    Chen, Fenghua
    [J]. VIBRATIONAL SPECTROSCOPY, 2024, 130
  • [3] Low- versus Mid-frequency Raman Spectroscopy for in Situ Analysis of Crystallization in Slurries
    Koskela, Jaana
    Sutton, Joshua J.
    Lipiainen, Tiina
    Gordon, Keith C.
    Strachan, Clare J.
    Fraser-Miller, Sara J.
    [J]. MOLECULAR PHARMACEUTICS, 2022, : 2316 - 2326
  • [4] Explanation and prediction for the crystallized products from amorphous bicalutamide and bicalutamide solutions by using mid-frequency Raman difference spectra
    Cheng, Xinyu
    Chen, Xiuzhi
    Liang, Chengfeng
    Jin, Hongjun
    Ren, Shizhao
    Xue, Rongrong
    Chen, Fenghua
    [J]. VIBRATIONAL SPECTROSCOPY, 2023, 127
  • [5] Evaporative Crystallization of Simvastatin from Different Solutions Using Mid-Frequency Raman Difference Spectra Explanations
    Chen, Xinyuan
    Chen, Xiuzhi
    Sun, Hongyan
    Li, Xiumin
    Ren, Shizhao
    Jin, Can
    Jin, Hongjun
    Chen, Fenghua
    Xue, Rongrong
    [J]. APPLIED SPECTROSCOPY, 2023, 77 (06) : 652 - 665
  • [6] Routes of Theophylline Monohydrate Dehydration Process Proposed by Mid-Frequency Raman Difference Spectra
    Ren, Shizhao
    Nian, Fanglin
    Chen, Xiuzhi
    Xue, Rongrong
    Chen, Fenghua
    [J]. JOURNAL OF PHARMACEUTICAL SCIENCES, 2023, 112 (11) : 2863 - 2868
  • [7] Direct comparison of low- and mid-frequency Raman spectroscopy for quantitative solid-state pharmaceutical analysis
    Lipiainen, Tiina
    Fraser-Miller, Sara J.
    Gordon, Keith C.
    Strachan, Clare J.
    [J]. JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2018, 149 : 343 - 350
  • [8] A prediction technique for dynamic analysis of flat plates in mid-frequency range
    Weicai Peng
    Zeng He
    Peng Li
    Jiaqiang Wang
    [J]. Acta Mechanica Solida Sinica, 2007, 20 : 333 - 341
  • [9] A PREDICTION TECHNIQUE FOR DYNAMIC ANALYSIS OF FLAT PLATES IN MID-FREQUENCY RANGE
    Weicai Peng Zeng He~* Peng Li Jiaqiang Wang (School of Civil Engineering and Mechanics
    [J]. Acta Mechanica Solida Sinica, 2007, (04) : 333 - 341
  • [10] A prediction technique for dynamic analysis of flat plates in mid-frequency range
    Peng, Weicai
    He, Zeng
    Li, Peng
    Wang, Jiaqiang
    [J]. ACTA MECHANICA SOLIDA SINICA, 2007, 20 (04) : 333 - 341
12345