Effect of C Addition on the Microstructure and Fracture Properties of In Situ Laminated Nb/Nb5Si3 Composites

被引:0
|
作者
Zeng, Delu [1 ]
Xiao, Lairong [1 ,2 ]
Xu, Shaofu [1 ]
Yu, Huali [1 ]
Zhang, Yu [1 ]
Yu, Chenxu [1 ]
Zhao, Xiaojun [1 ,2 ]
Cai, Zhenyang [1 ,2 ]
Li, Wei [3 ]
机构
[1] Cent South Univ, Sch Mat Sci & Engn, Changsha 410083, Peoples R China
[2] Cent South Univ, Key Lab Nonferrous Met Mat Sci & Engn, Minist Educ, Changsha 410083, Peoples R China
[3] Cent South Univ, Powder Met Res Inst, Changsha 410083, Peoples R China
基金
中国国家自然科学基金;
关键词
laminated Nb/Nb5Si3 composite; spark plasma sintering; orientation relationship; fracture toughness; compressive strength; MECHANICAL-PROPERTIES; OXIDATION RESISTANCE; HEAT-TREATMENT; NB; BEHAVIOR; ZR; HF;
D O I
10.3390/ma16165637
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
//Nb-ss and alpha-Nb5Si3 phases were detected. Meanwhile, Nb2C was observed, and the crystal forms of Nb5Si3 changed in the C-doped composites. Furthermore, micron-sized and nanosized Nb2C particles were found in the Nbss layer. The orientation relationship of Nb2C phase and the surrounding Nb-ss was [001](Nbss)//[010](Nb2C), (200) (Nbss)//(101) (Nb2C.) Additionally, with the addition of C, the compressive strength of the composites, at 1400 degrees C, and the fracture toughness increased from 310 MPa and 11.9 MPa .m(1/2) to 330 MPa and 14.2 MPa .m(1/2), respectively; the addition of C mainly resulted in solid solution strengthening.
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页数:13
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