Effects of Processing Variables on the Morphology and Microstructural Characteristics of TiO2 Fibers Produced by Solution Blow Spinning

被引：0
|
作者：
Leite, Raquel Santos [1 ]
Severo, Lucas Leite [2 ]
da Costa, Danubia Lisboa [3 ]
Farias, Rosiane Maria da Costa [1 ]
Santana, Lisiane Navarro de Lima [2 ]
Menezes, Romualdo Rodrigues [2 ]
Neves, Gelmires de Araujo [2 ]
机构：
[1] Univ Fed Campina Grande, Ctr Ciencias & Tecnol, Dept Engn Mat, BR-58428830 Campina Grande, PB, Brazil
[2] Univ Fed Campina Grande, Ctr Ciencias Tecnol, Programa Posgrad Ciencia & Engn Mat, BR-58428830 Campina Grande, PB, Brazil
[3] Inst Fed Paraiba, BR-58700000 Patos de Minas, PB, Brazil
来源：
MATERIALS RESEARCH-IBERO-AMERICAN JOURNAL OF MATERIALS | 2023年 / 26卷
关键词：
Solution blow spinning; Titanium dioxide; Fibers; Factorial design; SUBMICROMETRIC FIBERS; AQUEOUS-SOLUTION; NANOFIBERS; DYE; OPTIMIZATION; DEGRADATION; FERRITE; POLYMER; NANO;
D O I：
10.1590/1980-5373-MR-2023-0186
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A factorial design was used to evaluate the effects of processing variables on the morphology and microstructural characteristics of titanium dioxide (TiO2) fibers produced by solution blow spinning (SBS). For this, tests were carried out varying TiO2 precursor content, feed rate, air pressure, polymer, and solvent. The TTIP concentration and feed rate statistically influenced the average diameters of the PVC/TiO2 system. The proper combination between polymer and solvent enables the obtaining of TiO2 nanofibers with similar morphologies either using hydrophilic or hydrophobic polymer, however, fiber diameter is influenced by type of system (polymer/solvent) used. Only the anatase crystalline phase was found in the fibers with the PVC polymer and THF solvent, while two crystalline phases were obtained in the fibers with PVP and alcohol, anatase and rutile, indicating that the variation of the polymer and solvent influences the crystalline phases of the TiO2 fibers studied.
引用
收藏
页数：9
相关论文
共 50 条
  • [41] Fundamental properties and processing characteristics of TiO2 in films and coatings
    Lashway, W
    1997 POLYMERS, LAMINATIONS, & COATING CONFERENCE, BOOKS 1 AND 2, 1997, : 11 - 11
  • [42] Morphology and microstructural properties of TiO2 nanopowders doped with trivalent Al and Ga cations
    Depero, LE
    Marino, A
    Allieri, B
    Bontempi, E
    Sangaletti, L
    Casale, C
    Notaro, M
    JOURNAL OF MATERIALS RESEARCH, 2000, 15 (10) : 2080 - 2086
  • [43] Characteristics of hollow TiO2 fibers via replication of sisal fiber
    Li, Guangqin
    Liu, Chunyan
    Liu, Yun
    JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2007, 90 (04) : 1283 - 1285
  • [44] Morphology and microstructural properties of TiO2 nanopowders doped with trivalent Al and Ga cations
    L. E. Depero
    A. Marino
    B. Allieri
    E. Bontempi
    L. Sangaletti
    C. Casale
    M. Notaro
    Journal of Materials Research, 2000, 15 : 2080 - 2086
  • [45] Photoinduced effects in TiO2 nanocrystalline films with different morphology
    Djaoued, Yahia
    Ozga, K.
    Wojciechowski, A.
    Reshak, A. H.
    Robichaud, J.
    Kityk, I. V.
    JOURNAL OF ALLOYS AND COMPOUNDS, 2010, 508 (02) : 599 - 605
  • [46] TiO2 Nanotubes - Annealing Effects on Detailed Morphology and Structure
    Albu, Sergiu P.
    Tsuchiya, Hiroaki
    Fujimoto, Shinji
    Schmuki, Patrik
    EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 2010, (27) : 4351 - 4356
  • [47] CaO/Al2O3 based fibers produced by solution blow spinning as a potential bifunctional catalyst for sorption-enhanced steam methane reforming
    Silva, Thamyscira H. S.
    Cesario, Moises R.
    Gennequin, Cedric
    Abi-Aad, Edmond
    Silva, Vinicius D.
    Macedo, Daniel A.
    2020 11TH INTERNATIONAL RENEWABLE ENERGY CONGRESS (IREC), 2020,
  • [48] Densification and microstructural evolution of TiO2 films prepared by sol-gel processing
    Bockmeyer, Matthias
    Loebmann, Peer
    CHEMISTRY OF MATERIALS, 2006, 18 (18) : 4478 - 4485
  • [49] Effect of Processing Temperature on the Morphology and Crystal Structure of Anodic TiO2 Nanotubes
    Tayyaba Ghani
    Mohammad Mujahid
    Mazhar Mehmood
    Muhammad Ubaidullah
    Attaullah Shah
    Arshad Mahmood
    Journal of Electronic Materials, 2020, 49 : 1881 - 1888
  • [50] Effect of Processing Temperature on the Morphology and Crystal Structure of Anodic TiO2 Nanotubes
    Ghani, Tayyaba
    Mujahid, Mohammad
    Mehmood, Mazhar
    Ubaidullah, Muhammad
    Shah, Attaullah
    Mahmood, Arshad
    JOURNAL OF ELECTRONIC MATERIALS, 2020, 49 (03) : 1881 - 1888
12345