Synthesis, magnetic and dielectric properties of poly (m-phenylenediamine)/ZnNiFe2O4 nanocomposites

被引：3
|
作者：
Kumar, K. Sathish [1 ]
Sundaram, K. [1 ]
Anand, Siddeswaran [2 ]
Vijayalakshmi, M. [3 ]
Logesh, M. [1 ]
Anbarasu, D. [1 ]
Asha, I. [1 ]
Kannapiran, Nagarajan [1 ,4 ]
机构：
[1] Karpagam Acad Higher Educ, Dept Chem, Coimbatore 641021, Tamil Nadu, India
[2] KSR Coll Technol, Dept Chem, Tiruchengode 637215, Tamil Nadu, India
[3] Nandha Engn Coll, Dept Chem, Erode 638052, Tamil Nadu, India
[4] Karpagam Acad Higher Educ, Adv Battery Res Ctr, Coimbatore 641021, Tamil Nadu, India
来源：
INORGANIC CHEMISTRY COMMUNICATIONS | 2024年 / 161卷
关键词：
PmPD; SEM; TEM; Dielectric constant; ZINC FERRITE; AC CONDUCTIVITY; NANOPARTICLES; POLY(O-PHENYLENEDIAMINE); PURE; SIZE;
D O I：
10.1016/j.inoche.2023.111983
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The different concentration of ZnNiFe2O4 nanoparticles dispersed Poly(m-phenylenediamine) (PmPD)/ZnNiFe2O4 nanocomposites were synthesized by in -situ chemical oxidative polymerization method and using auto combustion method for preparation of ZnNiFe2O4 nanoparticles. The synthesized PmPD/ZnNiFe2O4 nanocomposites were characterized by XRD, FTIR, SEM, TEM, TGA and VSM. The formation and crystalline size of PmPD/ZnNiFe2O4 nanocomposites were confirmed through XRD and FTIR. The surface, morphology and shape of the PmPD/ZnNiFe2O4 nanocomposites were studied by SEM and TEM. The concentration of ZnNiFe2O4 influenced the thermal stability of PmPD/ZnNiFe2O4 nanocomposites. The hysteresis loop of ZnNiFe2O4 and PmPD/ZnNiFe2O4 nanocomposites confirmed their ferromagnetic behaviour. The dielectric constant of samples was analysed with different temperatures and frequencies.
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页数：9
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