A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells

被引：4

作者：

Bussetti, Gianlorenzo ^{[1
]}

Menegazzo, Marco ^{[1
]}

Mitko, Sergei ^{[2
]}

Castiglioni, Chiara ^{[3
]}

Tommasini, Matteo ^{[3
]}

Lucotti, Andrea ^{[3
]}

Magagnin, Luca ^{[3
]}

Russo, Valeria ^{[4
]}

Li Bassi, Andrea ^{[4
]}

Siena, Martina ^{[5
]}

Guadagnini, Alberto ^{[5
]}

Grillo, Samuele ^{[6
]}

Del Curto, Davide ^{[7
]}

Duo, Lamberto ^{[1
]}

机构：

[1] Politecn Milan, Dept Phys, I-20133 Milan, Italy

[2] NT MDT BV, Hoenderpk Weg 96 B, NL-7335 GX Apeldoorn, Netherlands

[3] Politecn Milan, Dept Chem Mat & Chem Engn, I-20133 Milan, Italy

[4] Politecn Milan, Dept Energy, I-20133 Milan, Italy

[5] Politecn Milan, Dept Civil & Environm Engn, I-20133 Milan, Italy

[6] Politecn Milan, Dept Elect Informat & Bioengn, I-20133 Milan, Italy

[7] Politecn Milan, Dept Architecture & Urban Studies, I-20133 Milan, Italy

来源：

MATERIALS | 2023年 / 16卷 / 06期

关键词：

solid-liquid interface; HOPG intercalation; in situ AFM; Raman spectroscopy; INTERCALATION COMPOUNDS; GRAPHITE-INTERCALATION; TUNNELING-MICROSCOPY; ANION INTERCALATION; GRAPHENE;

D O I：

10.3390/ma16062239

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

An innovative and versatile set-up for in situ and real time measures in an electrochemical cell is described. An original coupling between micro-Raman spectroscopy and atomic force microscopy enables one to collect data on opaque electrodes. This system allows for the correlation of topographic images with chemical maps during the charge exchange occurring in oxidation/reduction processes. The proposed set-up plays a crucial role when reactions, both reversible and non-reversible, are studied step by step during electrochemical reactions and/or when local chemical analysis is required.

引用

页数：10

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