Structural, magnetic, and antibacterial activity of the pure, Zn-doped, and Zn-doped/sugar-assisted coprecipitation synthesized semicrystalline Co3O4 compound

被引:3
|
作者
Prameela, P. [1 ]
Ramya, J. Ramana [2 ]
Gajendiran, J. [1 ]
Gnanam, S. [3 ]
Ramachandran, K. [4 ]
Raj, S. Gokul [5 ]
Kumar, G. Ramesh [6 ]
机构
[1] Vel Tech Rangarajan Dr Sagunthala R&D Inst Science, Dept Phys, Chennai 600062, India
[2] Saveetha Dent Coll & Hosp, Saveetha Inst Med & Tech Sci SIMATS, Dept Periodont, Chennai 600077, India
[3] Vels Inst Sci Technol & Adv Studies VISTAS, Sch Basic Sci, Dept Phys, Chennai 600117, India
[4] SRMIST, Dept Phys, Chennai 600026, India
[5] C Kandaswami Naidu Coll Men, Dept Phys, Chennai 600102, India
[6] Anna Univ Chennai, Univ Coll Engn Arni, Dept Sci & Humanities, Arni 632326, India
关键词
Semicrystalline material; Structural properties; Magnetic properties; Antibacterial activity; COBALT OXIDE NANOPARTICLES; THERMAL-DECOMPOSITION; COMPLEX;
D O I
10.1016/j.molstruc.2023.136154
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Undoped, Zn-doped, and Zn-doped/sugar-assisted semi-crystalline structures of Co3O4 were made by introducing a facile precipitation approach. The synthesized compounds were tested for surface characteristics, magnetic properties, and antibacterial activity. Powder X-ray diffraction (XRD) analysis confirmed semi-crystalline behavior and spinel structure formation in all synthesized compounds. Using scanning electron microscopy (SEM) characterization, microstructure formation along with the large agglomeration of spherical particles, uniform distribution of spherical particles, and spherical-flake-like particle structures were noticed for the pure, Zn-doped, and Zn-doped/sugar-assisted Co3O4 samples, respectively. From the vibration sample magnetometry (VSM), Zn-doped/sugar-assisted Co3O4 was found to have relatively lower saturation magnetization when compared to pure Co3O4 and Zn-doped Co3O4 material. The antibacterial performance of the synthesized compounds against the bacteria Escherichia coli (E.coli) and Staphylococcus aureus (S. aureus) has been tested. The above-mentioned germicidal responses showed a relatively larger inhibition zone for the Zn-doped and Zndoped/sugar-assisted Co3O4 compared to the undoped Co3O4 sample. The obtained diameter inhibition zone values of all synthesised compounds are comparable to the standard positive and negative control.
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页数:8
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