Determination of Trace Perfluoroalkyl Acids (PFAAs) in Soil by Chelating Resin-Assisted Extraction and High-Performance Liquid Chromatography - Mass Spectrometry (HPLC-MS)

被引：1
|
作者：
Li, Chenghua [1 ]
Wang, Yan [1 ]
Liu, Jinsong [2 ,3 ]
Huang, Guoliang [1 ]
Zhang, Baoshan [1 ]
Jiang, Kezhi [1 ,4 ]
机构：
[1] Hangzhou Normal Univ, Coll Mat Chem & Chem Engn, Key Lab Organosilicon Chem & Mat Technol, Minist Educ, Hangzhou, Peoples R China
[2] Zhejiang Ecol & Environm Monitoring Ctr, Zhejiang Key Lab Ecol & Environm Monitoring Forewa, Hangzhou, Peoples R China
[3] Zhejiang Ecol & Environm Monitoring Ctr, Zhejiang Key Lab Ecol & Environm Monitoring Forewa, Xueyuan Rd 117, Hangzhou, Peoples R China
[4] Hangzhou Normal Univ, Coll Mat Chem & Chem Engn, Key Lab Organosilicon Chem & Mat Technol, Minist Educ, Yuhangtang Rd 2318, Hangzhou, Peoples R China
来源：
ANALYTICAL LETTERS | 2024年 / 57卷 / 10期
关键词：
Chelating resin; high-performance liquid chromatography - mass spectrometry (HPLC-MS); perfluoroalkyl acids (PFAAs); perfluorocarboxylic acid; perfluorosulfonic acid; soil analysis; PERFLUOROCARBOXYLIC ACIDS; SUBSTANCES PFAS; MICROEXTRACTION; DISTRIBUTIONS; WATER;
D O I：
10.1080/00032719.2023.2257341
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Perfluoroalkyl acids (PFAAs) are widely distributed persistent organic pollutants and their monitoring in environmental media has received extensive attention. The soil matrix is complex, and efficient and simple extraction of PFAAs remains a challenge for analysts. In this work, a simple and rapid method has been developed for the determination of 21 PFAAs in soil by chelating resin-assisted extraction combined with high-performance liquid chromatography - mass spectrometry (HPLC-MS). Treatment with chelating resins effectively released PFAAs bound to metal ions, thereby greatly improving the extraction efficiency of PFAAs in soil. The complete extraction procedure only required 30 min. Under the optimized conditions, the quantification limits of the 21 PFAAs were from 0.03 to 0.49 ng/mL. Single PFAAs were detected in soil samples with concentrations ranging from 0.10 to 2.60 ng/g and recoveries between 70 and 126%.
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收藏
页码：1515 / 1525
页数：11
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