Mechanical Properties and Ion Release from Fibre-Reinforced Glass Ionomer Cement

被引:2
|
作者
Ivica, Anja [1 ]
Salinovic, Ivan [1 ]
Jukic Krmek, Silvana [1 ]
Garoushi, Sufyan [2 ,3 ]
Lassila, Lippo [2 ,3 ]
Saeilynoja, Eija [2 ,3 ,4 ]
Miletic, Ivana [1 ]
机构
[1] Univ Zagreb, Sch Dent Med, Dept Endodont & Restorat Dent, Zagreb 10000, Croatia
[2] Univ Turku, Inst Dent, Dept Biomat Sci, Turku 20520, Finland
[3] Univ Turku, Inst Dent, Turku Clin Biomat Ctr TCBC, Turku 20520, Finland
[4] Stick Tech Ltd, Res Dev & Prod Dept, Turku, Finland
关键词
glass fibres; glass ionomer cements; fluoride release; reinforcement; PHYSICAL-PROPERTIES; FLUORIDE RELEASE; COMPOSITE; MICROHARDNESS; RESTORATIONS; STRENGTH;
D O I
10.3390/polym16050607
中图分类号
O63 [高分子化学(高聚物)];
学科分类号
070305 ; 080501 ; 081704 ;
摘要
The aim of this study was to compare the mechanical properties and ion release from a commercially available resin-modified glass ionomer cement to a formulation reinforced by the addition of short glass fibres at various percentages. Methods: Three experimental groups were prepared by adding a mass ratio of 10%, 15% and 20% of short glass fibres to the powder portion of the cement from a capsule (GC Fuji II LC), while the control group contained no fibres. Microhardness (n = 12), fracture toughness, and flexural, compressive and diametral tensile strength (n = 8) were evaluated. To study ion release, readings were obtained utilising fluoro-selective and calcium-selective electrodes after 24 h, 7 days and 30 days (n = 12). The spatial distribution of fibres within the material was evaluated through scanning electron microscopy. The data were analysed using one-way ANOVA with a Bonferroni adjustment. Results: The findings suggest that elevating fibre weight ratios to 20 wt% results in improved mechanical properties (p < 0.05) in microhardness, flexural strength, diametral tensile strength and fracture toughness. In terms of ion release, a statistically significant difference (p < 0.001) was observed between the groups at the conclusion of 24 h and 7 days, when the fluoride release was much higher in the control group. However, after 30 days, no significant distinction among the groups was identified (p > 0.05). Regarding calcium release, no statistically significant differences were observed among the groups at any of the evaluated time points (p > 0.05). SEM showed the fibres were homogeneously incorporated into the cement in all experimental groups. Conclusions: Resin-modified glass ionomer enhanced with short glass fibres at a weight loading of 20% showcased the most favourable mechanical properties while concurrently maintaining the ability to release fluoride and calcium after a 30-day period.
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页数:12
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