The Effect of Changes in the Aging Temperature Combined with Deep Cryogenic Treatment on the Structure, Phase Composition, and Micromechanical Properties of the WE43 Magnesium Alloy

被引:3
|
作者
Barylski, Adrian [1 ]
Aniolek, Krzysztof [1 ]
Dercz, Grzegorz [1 ]
Matula, Izabela [1 ]
Rak, Jan [1 ]
Mazur, Izabela [1 ]
机构
[1] Univ Silesia Katowice, Inst Mat Engn, Fac Sci & Technol, 75 Pulku Piechoty St 1A, PL-41500 Chorzow, Poland
关键词
WE43 magnesium alloy; solution treatment; aging; deep cryogenic treatment; microstructure; XRD; EDS; instrumental indentation; IN-VIVO CORROSION; MECHANICAL-PROPERTIES; MICROSTRUCTURE; BEHAVIOR;
D O I
10.3390/ma16237447
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
This paper examines the optimal aging temperature of WE43 alloy that has undergone precipitation hardening in conjunction with deep cryogenic treatment. The microstructure and phase composition were investigated, a microanalysis of the chemical composition was performed, and instrumental indentation tests were performed to determine the parameters of the micro-mechanical properties of the alloy after different heat treatment variants. It has been proven that a decrease in the aging temperature from 250 degrees C to 225 degrees C and the introduction of a deep cryogenic treatment lead to favorable changes in the microstructure of the alloy (reduction in grain size, increase in the number, and change in the type of beta-phase precipitates). The changes in the alloy structure achieved by lowering the aging temperature contribute to the improvement of the micromechanical properties of the test material. The most advantageous results were recorded for an alloy subjected to solution treatment and aged at 225 degrees C for 24 h with deep cryogenic treatment: a 30% increase in hardness, a 10% increase in Young's modulus, an improvement in elastic properties, and increased resistance to deformation of the alloy were shown compared to the initial (as-received) state. Raising the aging temperature to 250 degrees C leads to a phenomenon known as alloy overaging for both alloys after classical precipitation hardening and after deep cryogenic treatment. The results indicate the significant effectiveness of the proposed heat treatment in improving the service life of the Mg-Y-Nd-Zr (WE43) alloy.
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页数:15
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