Synthesis and Crystal Structure of Zn(II) Complex with Tridentate Ligand N-(2-Hydroxy-1-naphthylidene)-L-serine

被引：0
|
作者：
YU Qing LI Chun-Ying BIAN He-Dong HUANG Fu-Ping LIANG Hong ② (College of Chemistry and Chemical Engineering
机构：
来源：
结构化学 | 2006年 / 08期
关键词：
Schiff base; Zn(II) complex; crystal structure;
D O I：
10.14102/j.cnki.0254-5861.2006.08.005
中图分类号：
O621.25 [];
学科分类号：
摘要：
A new Zn(II) complex, [Zn(L)2(H2O)2], where H2L = N-(2-hydroxy-1-naphthyli- dene)-L-serine, has been synthesized and characterized by single-crystal X-ray diffraction. The crystal belongs to monoclinic system, space group C2/c with a = 13.669(2), b = 6.4657(9), c = 31.463(5) ?, β = 98.010(2)o, V = 2753.6(7) ?3, Z = 8, Mr = 358.64, Dc = 1.730 g/cm3, F(000) = 1472, μ(MoKα) = 1.814 mm–1, the final R = 0.0355 and wR = 0.0706. The Zn(II) atom adopts a square-pyramidal geometry coordinated by the tridentate ligand and two water molecules. Intermolecular hydrogen bonds link the complex molecules into a two-dimensional layer.
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页码：915 / 918
页数：4
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