SYNTHESIS AND CHARACERIZATION OF LADDER-LIKE POLYDECYLSILSESQUIOXANE

被引：0

作者：

戴道荣

机构：

[1] Beijing 100080

[2] China Polymer Chemistry Laboratory

[3] Chinese Academy of Sciences

[4] Chinese Academy of Sciences and China Petrochemical Corporation

[5] Institute of Chemistry

[6] PCLCC

来源：

Chinese Journal of Polymer Science | 1999年 / 01期

基金：

中国国家自然科学基金;

关键词：

Ladder-like polydecylsilsesquioxane; Preamminolysis reaction;

D O I：

暂无

中图分类号：

TQ317 [高分子化合物产品];

学科分类号：

摘要：

Ladder-like polydecylsilsesquioxane （LPDS） was synthesized by a preamminolysis reaction ofdecyltrichlorosilane with ethylene diamine, followed by hydrolysis and polycondensation reaction. LPDS issoluble in a nonpolar solvent such as heptane and insoluble in a high polar solvent such as methanol. It wascharaterized by IR,;H-NMR,;Si-NMR, GPC and X-ray diffraction.

引用

页码：71 / 74

页数：4

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