SYNTHESIS AND STRUCTURE OF [4Ni（SALEN）·GGH] CLO4· EtOH·H2O （GG=Glycylglyciae）

被引：0
|
作者：
Zi Ming SUN-(?)
机构：
来源：
ChineseChemicalLetters | 1991年 / 10期
关键词：
EtOH; H2O; GG=Glycylglyciae; SALEN; GG; CLO4; GGH; Ni;
D O I：
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学科分类号：
摘要：
The complex of [4Ni（salen）·GGH] CLO;·EtOH·H;O has been synthesized and studied by X-ray single crystal analysis. The results show that there are both intra-unit hydrogen bonds in the [4Ni（salen）·GGH];and inter-unit hydrogen bonds between the two [4Ni（salen）·GGH];. Ni（salen） in the unit are still centrosymmetric dimers with planar structure. Imide N（10）—H（10） in the [GGH];bonds with one phenolic oxygen 0（7） of Ni（salen） dimer in the same unit. Two H atoms of amino group N（9）— H [H（A）, H（C）] in the glycylglycine perchlorate interact with phenolic oxygen [0（3）, 0（5）] of [4Ni（salen）·GGH];through two strong hydrogen bonds respectively.
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页码：781 / 782
页数：2
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