Hydrothermal Synthesis and Crystal Structure of a New Phosphonate:{[Cu(1,10-phen)]2-(H2O3PCH2C6H4C6H4CH2PO3H)2-(HO3PCH2C6H4C6H4CH2PO3H)}n

被引：0
|
作者：
FU Rui-Biao WU Xin-Tao② HU Sheng-Min WANG Long-Sheng(State Key Laboratory of Structural Chemistry
机构：
来源：
Chinese Journal of Structural Chemistry | 2004年 / 10期
关键词：
hydrothermal synthesis; single crystal; phosphonate;
D O I：
10.14102/j.cnki.0254-5861.2004.10.004
中图分类号：
O627.51 [磷有机化合物];
学科分类号：
070303 ; 081704 ;
摘要：
A new stepping chain {[Cu(1,10-phen)]2(H2O3PCH2C6H4C6H4CH2PO3H)2(HO3P- CH2C6H4C6H4CH2PO3H)}n 1 (C66H60Cu2N4O18P6) has been hydrothermally synthesized and charac- terized by single-crystal X-ray diffraction. It belongs to monoclinic, space group C2/c with a = 25.6114(4), b = 18.3781(2), c = 16.5180(3) ? b = 124.0610(10)? V = 6441.00(17) ?, Z = 4, Dc = 1.557 g/cm3, m(Mo-Ka) = 0.887 mm-1, F(000) = 3104, the final R = 0.0853 and wR = 0.1676 for 5585 independent reflections.
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页码：1107 / 1110 +1089
页数：5
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