A Facile Synthetic Method for Biphenyltetracarboxylic Dianhydrides

被引：0
|
作者：
Xue E WU
机构：
来源：
ChineseChemicalLetters | 2004年 / 07期
关键词：
Biphenyltetracarboxylic dianhydrides; nickel-catalyzed; electroreductive coupling;
D O I：
暂无
中图分类号：
O621 [有机化学一般性问题];
学科分类号：
070303 ; 081704 ;
摘要：
We report a facile and high-yielding procedure for preparing biphenyltetracarboxylic dianhydrides (BPDAs). This method relies on a nickel-catalyzed electroreductive coupling reaction of dimethyl 3-chorophthalate (3-DMCP) and/or dimethyl 4-chorophthalate (4-DMCP) with subsequent hydrolysis of tetra-ester and dehydration of tetra-acid.
引用
收藏
页码：787 / 790
页数：4
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