Microwave-Assisted Synthesis of Poly(Aspartic Acid-Itaconic Acid) Copolymer and Its Characterization

被引：0
|
作者：
Zhang Yuling [1 ]
Jiang Yijian [1 ]
Hu Zhiguang [1 ]
Wei Hanxiao [1 ]
Guo Jun [2 ]
Wang Jilong [1 ]
机构：
[1] Department of Environmental Science & Engineering, North China Electric Power University
[2] Department of Computer, North China Electric Power University
来源：
China Petroleum Processing & Petrochemical Technology | 2016年 / 18卷 / 03期
基金：
中国国家自然科学基金; 中央高校基本科研业务费专项资金资助;
关键词：
aspartic acid; itaconic acid; copolymerization; scale inhibition;
D O I：
暂无
中图分类号：
TQ317 [高分子化合物产品];
学科分类号：
0805 ; 080502 ;
摘要：
Poly（aspartic acid-itaconic acid） copolymer was synthesized from aspartic acid（Asp） and itaconic acid（Ita） under microwave irradiation. The effects of microwave power, microwave irradiation time, molar ratio of itaconic acid and aspartic acid, catalyst type, catalyst and organic solvent content on copolymer yield, and the performance for inhibition of CaCO;fouling were investigated. It was found that the product yield achieved a highest record of 95% when the amount of catalyst Na H;PO;was 0.012 mol, the amount of organic solvent propylene carbonate was 16 m L, the molar ratio of Asp/Ita was 3:1, the microwave output power was 1200 W and the irradiation time was 5.5 min. And the product performance for inhibition of calcium carbonate also reached a highest value of 94.38%. Structural characterization of the product showed that the product was the aspartic acid-itaconic acid copolymer.
引用
收藏
页码：76 / 82
页数：7
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