LC-MS/MS analysis and validation of pesticides residue in vegetables asserted to be organic

被引:0
|
作者
Rad, Raluca [1 ,2 ]
Costea, Liana Maria [3 ]
Meghesan, Adela [1 ]
Cimpoiu, Claudia [1 ,2 ]
机构
[1] Babes Bolyai Univ, Fac Chem & Chem Engn, Cluj Napoca, Romania
[2] Res Ctr Adv Chem Anal Instrumentat & Chemometr, Cluj Napoca, Romania
[3] 1 Decembrie 1918 Univ Alba Iulia, Fac Law & Social Sci, Alba Iulia, Romania
关键词
LC-MS/MS method; organic vegetables; pesticides residues; validation;
D O I
10.1080/10826076.2025.2479790
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
The term pesticides refers to a huge group of compounds (over 1000 substances) that have diverse chemical characters and are found in vegetables in a wide range of concentrations. For this reason, pesticide residue analysis is an important task in order to protect human health. A simple and reproducible analytical method has been developed to simultaneously determination of 35 major pesticides residues in vegetables. Following the analysis of 160 vegetable samples harvested in 2023 and 2024, it was found that around 40% of them contained pesticide residues. In some cases, limits were exceeded, even for organic pesticides, and in other cases, residues of obsolete pesticides were detected. Concluding, the level of pesticide residues in vegetables grown in greenhouses or solariums, even if purchased from local producers, can be harmful.
引用
收藏
页数:12
相关论文
共 50 条
  • [41] Investigation of neonicotinoid pesticides in Slovenian honey by LC-MS/MS
    Mrzlikar, Miha
    Heath, David
    Heath, Ester
    Markelj, Jernej
    Borovsak, Andreja Kandolf
    Prosen, Helena
    LWT-FOOD SCIENCE AND TECHNOLOGY, 2019, 104 : 45 - 52
  • [42] Analysis of isocyanates with LC-MS/MS
    Östin, A
    Sundgren, M
    Ekman, J
    Lindahl, R
    Levin, JO
    ISOCYANATES: SAMPLING, ANALYSIS, AND HEALTH EFFECTS, 2001, 1408 : 12 - 20
  • [43] Analysis of neurotransmitters with LC-MS/MS
    Uutela, P
    Piepponen, P
    Kotiaho, T
    Kostiainen, R
    EUROPEAN JOURNAL OF PHARMACEUTICAL SCIENCES, 2003, 19 : S32 - S33
  • [44] LC-MS/MS analysis of chitooligosaccharides
    Kim, Jaehyun
    Kim, Jinhee
    Hong, Jangmi
    Lee, Sunyoung
    Park, Sehwan
    Lee, Ji-Hye
    Kim, Jeongkwon
    CARBOHYDRATE RESEARCH, 2013, 372 : 23 - 29
  • [45] LC-MS/MS Analysis of Choline Compounds in Japanese-Cultivated Vegetables and Fruits
    Wang, Wenhao
    Yamaguchi, Shohei
    Koyama, Masahiro
    Tian, Su
    Ino, Aya
    Miyatake, Koji
    Nakamura, Kozo
    FOODS, 2020, 9 (08)
  • [46] Determination of nitenpyram dissipation and residue in kiwifruit by LC-MS/MS
    Ge, Shijia
    Wang, Ye
    Song, Qingmei
    Chen, Lingzhu
    Zhang, Yuping
    Hu, Deyu
    FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT, 2020, 37 (06): : 955 - 962
  • [47] Analysis of biopharmaceutical proteins in biological matrices by LC-MS/MS II. LC-MS/MS analysis
    Hopfgartner, Gerard
    Lesur, Antoine
    Varesio, Emmanuel
    TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2013, 48 : 52 - 61
  • [48] Method development and validation of cabozantinib by LC-MS/MS
    Venkateshwarlu, Punna
    Patel, Mehul M.
    PHARMACIA, 2022, 69 (02) : 407 - 413
  • [49] Validation of a global method for the simultaneous analysis of polar and non-polar pesticides by online extraction and LC-MS/MS
    Piovesana, Susy
    Aita, Sara Elsa
    Cavaliere, Chiara
    Cerrato, Andrea
    Lagana, Aldo
    Montone, Carmela Maria
    Taglioni, Enrico
    Capriotti, Anna Laura
    ANALYTICA CHIMICA ACTA, 2024, 1329
  • [50] Validation Study on a Rapid Method for Simultaneous Determination of Pesticide Residues in Vegetables and Fruits by LC-MS/MS
    Sato, Tamaki
    Miyamoto, Iori
    Uemura, Masako
    Nakatani, Tadashi
    Kakutani, Naoya
    Yamano, Tetsuo
    FOOD HYGIENE AND SAFETY SCIENCE, 2016, 57 (04): : 107 - 115