POLYBORATE SUPPORTED PERCHLORIC ACID AS AN EFFICIENT SOLID ACID CATALYST FOR ONE-POTSYNTHESIS OF 12-ARYL-8, 9, 10, 12TETRAHYDROBENZO[A]XANTHENE-11-ONE DERIVATIVES UNDER SOLVENT-FREE CONDITION

被引：0

作者：

Aute, Dilip ^{[1
]}

Bendre, Tushar ^{[1
]}

Parhad, Amol ^{[1
]}

Murade, Vaishali ^{[1
]}

Shirole, Gopinath ^{[2
]}

Kadnor, Vijay ^{[3
]}

Uphade, Bhagwat ^{[1
]}

Gadhave, Anil ^{[1
]}

机构：

[1] Savitribai Phule Pune Univ, Padmashri Vikhe Patil Coll, Dept Chem & Res Ctr, Pune 413736, Maharashtra, India

[2] Arts Sci & Commerce Coll, Dept Chem, Rahata, India

[3] Arts Commerce & Sci Coll, Dept Chem, Satral, India

来源：

HETEROCYCLIC LETTERS | 2024年 / 14卷 / 01期

关键词：

Multi-component reaction; perchloric polyborate; solvent-free conditions; green chemistry; xanthenes; ONE-POT SYNTHESIS; PROMOTED ONE-POT; GREEN SYNTHESIS; PROTOCOL; 1,8-DIOXO-OCTAHYDROXANTHENES; SCAFFOLDS; VERSATILE; FACILE; PYRAN;

D O I：

暂无

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

In the present study, perchloric acid supported on polyborate catalyst was subjected for the synthesis of 12-aryl-8,9,10,12-tetrahydrobenzo[a]xanthene-11-one derivatives by one-pot, three-component reaction between aromatic aldehydes, 2-naphtholanddimedone under solvent- free condition. Superiority of the present protocol includes short reaction time, solvent-free condition, excellent yield, high purity, cleaner reaction profiles, easy set-up, mild reaction condition and straightforward experimental procedures. The prepared perchloric polyborate solid acid catalyst was characterized by analytical techniques like energy dispersive x-ray analysis, x-ray diffraction, field emission scanning electron microscopy and flourier transform infrared spectroscopy analysis.

引用

页码：153 / 168

页数：16

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