Comparison of three extraction methods, DMU-SPME, SAFE, and SDE, for the analysis of flavor compounds in soy sauce

被引：0
|
作者：
Ma, Yun-Jiao [1 ,2 ]
Bi, An-Qi [1 ]
Li, Ping [1 ]
Zhu, Bei-Wei [1 ]
Du, Ming [1 ]
Xu, Xian-Bing [1 ]
机构：
[1] Dalian Polytech Univ, SKL Marine Food Proc & Safety Control, Collaborat Innovat Ctr Seafood Deep Proc, Sch Food Sci & Technol,Natl Engn Res Ctr Seafood, Dalian 116034, Peoples R China
[2] Liaoning Agr Vocat & Tech Coll, Yingkou 115009, Peoples R China
来源：
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES | 2025年 / 1256卷
关键词：
Dual mode unity solid-phase microextraction; Solvent assisted flavor evaporation; Simultaneous distillation extraction; Volatile organic compounds; SOLID-PHASE MICROEXTRACTION; SIMULTANEOUS DISTILLATION-EXTRACTION; GAS-CHROMATOGRAPHY; VOLATILE COMPOUNDS; TRAP EXTRACTION; EVAPORATION; AROMA;
D O I：
10.1016/j.jchromb.2025.124562
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
The dual mode unity solid-phase microextraction (DMU-SPME) was evaluated against traditional solvent-based methods, including solvent-assisted flavor evaporation (SAFE) and simultaneous distillation extraction (SDE), to explore its potential as an alternative. Compared to SAFE and SDE, DMU-SPME is a green extraction technology for volatile organic compounds. The results demonstrated that DMU-SPME significantly outperformed both SAFE and SDE in extracting medium-volatility compounds (retention time of 20-40 min), identifying 55 unique volatiles. With the exception of hydrocarbons, DMU-SPME exhibited superior extraction efficiency and significantly better stability compared to both SAFE and SDE methods. Thus, DMU-SPME proves to be a promising alternative for the comprehensive extraction of volatile organic compounds.
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页数：10
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